期刊
ADVANCED SYNTHESIS & CATALYSIS
卷 360, 期 9, 页码 1861-1869出版社
WILEY-V C H VERLAG GMBH
DOI: 10.1002/adsc.201800136
关键词
Aldehydes; Fluorides; Radical reactions; Synthetic methods; Monofluoromethylthioesters
资金
- Natural Science Basic Research Plan in Shaanxi Province of China [2017JM2006]
- National Natural Science Foundation of China [NSFC-21572178, NSFC-21702162]
- Key Science and Technology Innovation Team of Shaanxi Province [2017KCT-37]
A direct and efficient approach to the synthesis of monofluoromethylthioesters from aldehydes has been developed. The synthetic method features mild reaction conditions, good tolerance of functional groups, a broad substrate scope, and especially no metal involved in the reaction. The approach has the potential to be an important tool for the late-stage functionalization of advanced synthetic intermediates, and may find many applications in medicinal chemistry.
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