期刊
ADVANCED SYNTHESIS & CATALYSIS
卷 353, 期 9, 页码 1474-1478出版社
WILEY-V C H VERLAG GMBH
DOI: 10.1002/adsc.201100113
关键词
alkynes; C-C bond formation; dienes; halopalladation; palladium
资金
- National Natural Science Foundation of China [20902084]
- RF for ROCS of SEM
- Science and Technology Office in Zhejiang Province [2010R10016]
A highly efficient and stereoselective method for the synthesis of (1Z)-1,2-dihalo-3-vinyl-1,3-dienes featuring palladium-catalyzed coupling of haloalkynes and 2,3-butadienyl acetates was developed. The resulting products were smoothly converted into cis-1,2-dihalostyrene derivatives using the Diels-Alder/aromatization sequence.
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