期刊
ADVANCED SYNTHESIS & CATALYSIS
卷 351, 期 5, 页码 733-737出版社
WILEY-V C H VERLAG GMBH
DOI: 10.1002/adsc.200800784
关键词
iodine; iodosylbenzene; 2-iodylbenzoic acid isopropyl ester (IBX-ester); oxygenation; porphyrins
资金
- National Science Foundation [CHE-0702734]
- Petroleum Research Fund [PRF-45510-GB-3]
A comparative study of the reactivity of 2-iodylbenzoic acid isopropyl ester (IBX-ester), oligomeric iodosylbenzene sulfate [(PhIO)(3)center dot SO3](n), and iodosylbenzene in the oxygenation of anthracene in the presence of metal porphyrin or phthalocyanine complexes is reported. Results of this study demonstrate that oligomeric iodosylbenzene sulfate and the IBX-ester are the most reactive oxygenating reagents that can be used as a safe and convenient alternative to the thermally unstable and potentially explosive iodosylbenzene.
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