4.7 Article

Comparison between superplastic deformation mechanisms at primary and steady stages of the fine grain AA7475 aluminium alloy

出版社

ELSEVIER SCIENCE SA
DOI: 10.1016/j.msea.2018.01.102

关键词

Superplasticity; Aluminium alloy; Grain structure; Dislocation structure; Mechanisms of deformation; Grain boundary sliding; Diffusion creep

资金

  1. Russian Science Foundation [17-79-20426] Funding Source: Russian Science Foundation

向作者/读者索取更多资源

Evolution of the deformation behaviour, surface and bulk structures at superplastic flow of the AA7475 aluminium-based alloy were studied by scanning and transmission electron microscopes and a focused ion beam technique. Differences between deformation behaviour at a primary stage with strains below 0.69 and a steady stage with strains above 0.69 were discussed. The research showed the grain growth and grain elongation to the stress direction at a primary stage of deformation. Stabilisation of both mean grain size and grain aspect ratio was found at a steady stage of deformation. Grain neighbour switching, grain rotation, dispersoid free zones and some insignificant intragranular strain were observed at both stages. Appearing and disappearing of the grains on the sample surface, with increased dislocation activity occurred at the steady stage of deformation. The current results highlighted the importance of diffusion creep as a dominant mechanism at the beginning of superplastic deformation and as an accommodation mechanism of the grain boundary sliding at the steady stage of deformation. The dislocation creep as an additional accommodation mechanism of the grain boundary sliding at the steady stage of superplastic deformation is suggested.

作者

我是这篇论文的作者
点击您的名字以认领此论文并将其添加到您的个人资料中。

评论

主要评分

4.7
评分不足

次要评分

新颖性
-
重要性
-
科学严谨性
-
评价这篇论文

推荐

Article Materials Science, Multidisciplinary

Fabrication of AA2024/SiCp Metal Matrix Composite by Mechanical Alloying

O. V. Rofman, A. S. Prosviryakov, A. D. Kotov, A. I. Bazlov, P. O. Milovich, Gopalu Karunakaran, A. V. Mikhaylovskaya

Summary: In this research, high-energy ball milling was used to disperse various volume fractions of sub-micron-sized SiCp particles in AA2024 aluminum powder alloy, focusing on powder morphology and milling conditions. Changes in lattice parameters of the matrix alloy were observed after mechanical alloying. Compression testing at elevated temperatures showed sufficient ductility for thermomechanical processing.

METALS AND MATERIALS INTERNATIONAL (2022)

Article Chemistry, Physical

The influence of minor additions of Y, Sc, and Zr on the microstructural evolution, superplastic behavior, and mechanical properties of AA6013 alloy

M. Esmaeili Ghayoumabadi, A. G. Mochugovskiy, N. Yu Tabachkova, A. Mikhaylovskaya

Summary: This study aimed to improve the superplastic formability of Alloy AA6013 by refining its grain structure and controlling grain growth at elevated temperatures. Minor additions of Y, Sc, and Zr were considered. The results showed that the additions led to a noticeable refinement of the grain structure and the formation of dispersed particles. These effects inhibited recrystallization and dynamic grain growth, resulting in grain refinement and achieving superplasticity in the alloy.

JOURNAL OF ALLOYS AND COMPOUNDS (2022)

Article Materials Science, Multidisciplinary

Microstructure, superplasticity, and mechanical properties of Al-Mg-Er-Zr alloys

A. D. Kotov, A. G. Mochugovskiy, A. O. Mosleh, A. A. Kishchik, O. V. Rofman, A. V. Mikhaylovskaya

Summary: Minor additions of rare-earth elements have been found to enhance the mechanical properties of aluminum-based alloys by improving precipitation strengthening and increasing resistance to recrystallization. This study investigated the microstructure, mechanical properties, and superplasticity of Al-Mg-Z-Er alloys with varying Mg content. The results showed that an increase in Mg content led to solid solution strengthening and facilitated dynamic recrystallization at high temperatures. The presence of fine L12 precipitates and (Al,Mg)3Er particles resulted in a fine-grained structure and excellent superplastic deformation behavior.

MATERIALS CHARACTERIZATION (2022)

Article Materials Science, Multidisciplinary

The effect of pre-straining on the annealing-induced precipitation behavior of the icosahedral I-phase in an aluminum-based alloy

A. G. Mochugovskiy, A. B. Mukhamejanova, A. D. Kotov, O. A. Yakovtseva, N. Yu Tabachkova, A. Mikhaylovskaya

Summary: The study reveals that pre-straining significantly accelerates the precipitation kinetics of Al-Mn-Mg alloy, increases the number density of quasicrystalline-structured precipitates, and induces a hardening effect after annealing.

MATERIALS LETTERS (2022)

Article Nanoscience & Nanotechnology

Influence of Fe on the microstructure, superplasticity and room-temperature mechanical properties of Ti-4Al-3Mo-1V-0.1B alloy

Anton D. Kotov, Maria N. Postnikova, Ahmed O. Mosleh, Anastasia Mikhaylovskaya

Summary: This study investigated the effect of Fe content on the microstructure, superplasticity, and post-forming mechanical properties of Ti-Al-Mo-V alloy. The results showed that increasing Fe content promoted recrystallization and fragmentation, leading to accelerated diffusivity. The alloys exhibited high strain rate sensitivity and maximum elongation to failure at a constant strain rate and low temperature. Alloying with Fe increased the post-forming room-temperature tensile strength and decreased ductility. Alloying with 0.5% Fe provided a good combination of superplastic and room-temperature mechanical properties.

MATERIALS SCIENCE AND ENGINEERING A-STRUCTURAL MATERIALS PROPERTIES MICROSTRUCTURE AND PROCESSING (2022)

Article Materials Science, Multidisciplinary

Microstructure and Superplastic Behavior of Ni-Modified Ti-Al-Mo-V Alloys

Anton D. Kotov, Maria N. Postnikova, Ahmed O. Mosleh, Vladimir V. Cheverikin, Anastasia Mikhaylovskaya

Summary: The paper investigates the effect of 0.5-1.8 wt.% Ni alloying on the superplasticity, microstructural evolution, and dynamic grain growth of two-phase Ti-Al-Mo-V alloys. The results show that an increase in Ni content significantly improves superplasticity, but excessive Ni content leads to a decrease in superplastic properties. The Ti-4Al-3Mo-1V-0.1B alloy with 0.9 wt.% Ni exhibits a good combination of superplastic behavior and room-temperature mechanical properties.

METALS (2022)

Article Chemistry, Physical

The influence of the Al2O3 particles on the microstructure of the mechanically alloyed Al-Mn-Cu alloy

Olga A. Yakovtseva, Andrey I. Bazlov, Alexey S. Prosviryakov, Nadezhda B. Emelina, Natalia Yu. Tabachkova, Anastasia V. Mikhaylovskaya

Summary: The microstructure, phase composition, and hardness evolutions of high-energy ball milled Al-15.3%Mn-6.2%Cu alloy and alloy matrix composites with 2% and 5% Al2O3 fine particles were investigated. The milling process dissolved the non-equilibrium phase CuAl2 and equilibrium phase Al20Cu2Mn3, resulting in a decrease in the lattice parameter and microhardness of aluminum. Further milling time and annealing of pre-milled samples led to the decomposition of the solid solution and precipitation of the Mn-enriched phase. The addition of Al2O3 particles refined the particles, increased the microhardness, and promoted the dissolution of phases and precipitation of the Mn-enriched phase, improving the precipitation hardening effect.

JOURNAL OF ALLOYS AND COMPOUNDS (2023)

Article Chemistry, Physical

Microstructure Evolution, Constitutive Modelling, and Superplastic Forming of Experimental 6XXX-Type Alloys Processed with Different Thermomechanical Treatments

Andrey G. Mochugovskiy, Ahmed O. Mosleh, Anton D. Kotov, Andrey V. Khokhlov, Ludmila Yu. Kaplanskaya, Anastasia V. Mikhaylovskaya

Summary: This study focused on the microstructural analysis, superplasticity, modeling of superplastic deformation behavior, and superplastic forming tests of the Al-Mg-Si-Cu-based alloy modified with Fe, Ni, Sc, and Zr. The effect of thermomechanical treatment on particle distribution and deformation behavior was studied. The constitutive model based on Arrhenius and Beckofen equations accurately described and predicted the superplastic flow behavior of the alloy, and the proposed strain rate provided high quality parts with low thickness variation.

MATERIALS (2023)

Article Materials Science, Multidisciplinary

Effect of Coarse Eutectic-Originated Particles on the Microstructure and Properties of the Friction Stir-Processed Al-Mg-Zr-Sc-Based Alloys

Ahmed O. Mosleh, Olga A. Yakovtseva, Anna A. Kishchik, Anton D. Kotov, Essam B. Moustafa, Anastasia V. Mikhaylovskaya

Summary: Friction stir processing (FSP) is a promising technique for refining grains and improving mechanical properties. This study compared an FSP-ed Al-Mg-Sc-Zr alloy with fine nanoscale Al-3(Sc,Zr) precipitates and an alloy modified with both Al-3(Sc,Zr) and coarse Al9FeNi-phase particles. The results showed that both secondary-phase particles and FSP parameters influenced the microstructure, mechanical properties, and superplasticity of the alloys. The modified alloy exhibited an improvement in ultimate tensile strength and elongation-to-fracture compared to the reference alloy, thanks to the effective grain refinement provided by the fine Al-3(Sc,Zr) and coarse Al9FeNi particles.
Article Nanoscience & Nanotechnology

Effect of Mo content on the microstructure, superplastic behavior, and mechanical properties of Ni and Fe-modified titanium alloys

Anton D. Kotov, Maria N. Postnikova, Ahmed O. Mosleh, Anastasia V. Mikhaylovskaya

Summary: The superplastic deformation behavior, strain-induced microstructure evolution, and post-deformation mechanical properties of Ti-4Al-1V-1Fe-1Ni-0.1B-xMo alloys (x = 1, 2.5, or 5 wt%) were investigated. It was found that 5% Mo content significantly improved the β-phase fraction, m-value, δ-value at low temperature (625°C), as well as the post-forming tensile mechanical properties at room temperature.

MATERIALS SCIENCE AND ENGINEERING A-STRUCTURAL MATERIALS PROPERTIES MICROSTRUCTURE AND PROCESSING (2023)

Article Chemistry, Physical

Effect of Boron on the Microstructure, Superplastic Behavior, and Mechanical Properties of Ti-4Al-3Mo-1V Alloy

Maria N. Postnikova, Anton D. Kotov, Andrey I. Bazlov, Ahmed O. Mosleh, Svetlana V. Medvedeva, Anastasia V. Mikhaylovskaya

Summary: The decrease of superplastic forming temperature and improvement of post-forming mechanical properties are important issues for titanium-based alloys. This study focuses on the influence of trace amounts of boron on the microstructure and properties of Ti-4Al-3Mo-1V alloys. The addition of 0.01-0.1wt.% boron significantly refines prior beta-grains and improves superplasticity.

MATERIALS (2023)

Article Materials Science, Multidisciplinary

Internal friction in AA5051 alloy subjected to compression with torsion

V. V. Palacheva, M. Yu. Zadorozhnyy, A. V. Mikhaylovskaya, P. A. Petrov, I. S. Golovin

Summary: Structural-induced anelasticity in AA5051 alloy was analyzed under two different treatment schemes: simple compression and compression combined with torsion. Anelasticity caused by structural transitions was studied using temperature, time, and amplitude-dependent tests. The sample subjected to compression combined with torsion exhibited a higher thermodynamical stimulus for recrystallization and higher dislocation density, resulting in a faster decrease in dislocation density during instant heating and isothermal annealing. The Avrami kinetics parameters for isothermal recrystallization and activation parameters for grain boundary relaxation after recrystallization were calculated.

MATERIALS LETTERS (2023)

Article Metallurgy & Metallurgical Engineering

The Microstructure and Mechanical Properties of Al-Mg-Fe-Ni-Zr-Sc Alloy after Isothermal Multidirectional Forging

A. A. Kishchik, S. A. Aksenov, M. S. Kishchik, D. O. Demin, A. Yu. Churyumov, A. V. Mikhaylovskaya

Summary: The effects of isothermal multidirectional forging (IMF) on the grain structure, second-phase particles of solidification origin, and dispersoids in the Al-4.9Mg-0.9Ni-0.9Fe-0.2Zr-0.1Sc alloy were investigated. The results showed that the strain distribution during forging has a significant influence on the alloy properties. A new method for constructing stress-strain curves was proposed to accurately characterize the mechanical behavior of the material. Additionally, increasing the number of phase cycles resulted in a reduction in the size of solidification-origin phase particles and a finer grain structure.

PHYSICS OF METALS AND METALLOGRAPHY (2023)

Article Nanoscience & Nanotechnology

The role of parent austenite grain size on the variant selection and intervariant boundary network in a lath martensitic steel

Ahmad Mirzaei, Peter D. Hodgson, Xiang Ma, Vanessa K. Peterson, Ehsan Farabi, Gregory S. Rohrer, Hossein Beladi

Summary: This study investigated the influence of parent austenite grain refinement on the intervariant boundary network in a lath martensitic steel. It found that refining the parent austenite grain led to a decrease in the fraction of certain boundaries in the martensite and an increase in the connectivity of low energy boundaries, ultimately improving the impact toughness.

MATERIALS SCIENCE AND ENGINEERING A-STRUCTURAL MATERIALS PROPERTIES MICROSTRUCTURE AND PROCESSING (2024)

Article Nanoscience & Nanotechnology

The interdependence of the thermal and mechanical cycling behaviour in Ti2448 (Ti-24Nb-4Zr-8Sn, wt%)

N. L. Church, C. E. P. Talbot, L. D. Connor, S. Michalik, N. G. Jones

Summary: Metastable beta Ti alloys based on the Ti-Nb system have attracted attention due to their unique properties. However, the unstable cyclic behavior of these alloys has hindered their widespread industrial use. Recent studies have shown that internal stresses, including those from dislocations, may be responsible for this behavior. This study demonstrates that inter-cycle thermal treatments can mitigate the unstable cyclic behavior, providing a significant breakthrough in our understanding of Ti-Nb superelastic materials.

MATERIALS SCIENCE AND ENGINEERING A-STRUCTURAL MATERIALS PROPERTIES MICROSTRUCTURE AND PROCESSING (2024)

Article Nanoscience & Nanotechnology

Ultrasonic-assisted soldering of SiC ceramic and aluminum alloy with a commercial inactive Sn3.0Ag0.5Cu solder

Di Zhao, Chenchen Zhao, Ziyang Xiu, Jiuchun Yan

Summary: This study proposes a novel strategy for achieving the bonding of SiC ceramic and Al alloy using ultrasound. The ultrasound promotes the dissolution of Al into the solder, activating the solder and triggering the interfacial reaction between SiC ceramic and solder. With increasing ultrasonic duration, the bonding between SiC and Al transitions from partial to full metallurgical bonding.

MATERIALS SCIENCE AND ENGINEERING A-STRUCTURAL MATERIALS PROPERTIES MICROSTRUCTURE AND PROCESSING (2024)

Article Nanoscience & Nanotechnology

Effect of grain orientation and precipitates on the superelasticity of Fe-Ni-Co-Al polycrystalline alloys

Kang Du, Yang Zhang, Guangda Zhao, Tao Huang, Liyuan Liu, Junpeng Li, Xiyu Wang, Zhongwu Zhang

Summary: This paper systematically investigated the evolution of microstructure in Fe-Ni-Co-Al polycrystalline alloys and its effects on mechanical properties. The results revealed that the migration of grain boundaries in different processes is driven by different factors, which impacts the grain orientation and precipitate formation. In the process of directional recrystallization, grains with specific orientations grow in the grain boundary region and form the dominant orientation, while grains with lower migration rate form the minor orientation. The alloy produced through directional recrystallization exhibited good recoverable strain and superelastic strain, while the alloy produced through solid solution treatment showed no evident superelastic behavior.

MATERIALS SCIENCE AND ENGINEERING A-STRUCTURAL MATERIALS PROPERTIES MICROSTRUCTURE AND PROCESSING (2024)

Article Nanoscience & Nanotechnology

Effect of thermomechanical processing on compressive mechanical properties of Ti-15Mo additively manufactured by laser metal deposition

Edohamen Awannegbe, Liang Chen, Yue Zhao, Zhijun Qiu, Huijun Li

Summary: This study employed laser metal deposition to additively manufacture Ti-15Mo wt% alloy, and subsequently subjected it to post-fabrication uniaxial thermomechanical processing. The results showed that different zones in the microstructure remained after processing, and deformation mechanisms mainly involved slip and martensite formation. The compressive mechanical properties were found to be dependent on strain rate, with higher flow stress and compressive strength observed at higher strain rates. Grain structure homogenisation was not achieved, leading to anisotropic tensile properties.

MATERIALS SCIENCE AND ENGINEERING A-STRUCTURAL MATERIALS PROPERTIES MICROSTRUCTURE AND PROCESSING (2024)

Article Nanoscience & Nanotechnology

Crystallographic texture and the mechanical properties of API 5L X70 pipeline steel designated for an arctic environment

Reza Khatib Zadeh Davani, Enyinnaya George Ohaeri, Sandeep Yadav, Jerzy A. Szpunar, Jing Su, Michael Gaudet, Muhammad Rashid, Muhammad Arafin

Summary: This research aims to investigate the effect of roughing and finishing reductions on crystallographic texture. The results show significant heterogeneity in the centerline region, with higher intensity of certain textures. Drop Weight Tear Test indicates that steel specimens with lower and medium reductions exhibit superior low-temperature impact toughness compared to steel with higher reductions. The electrochemical hydrogen charging experiments confirm the presence of internal hydrogen cracks only in steel with lower and medium reductions.

MATERIALS SCIENCE AND ENGINEERING A-STRUCTURAL MATERIALS PROPERTIES MICROSTRUCTURE AND PROCESSING (2024)

Article Nanoscience & Nanotechnology

Effect of Cr content in temperature-dependent mechanical properties and strain hardening of a twinning-induced plasticity steel

Flavio De Barbieri, Denis Jorge-Badiola, Rodrigo Allende, Karem Tello, Alfredo Artigas, Franco Perazzo, Henry Jami, Juan Perez Ipina

Summary: This study examines the effect of Cr additions on the mechanical behavior of TWIP steel at temperatures ranging from 25°C to 350°C. The results indicate that different temperature-dependent strengthening mechanisms, including mechanical twinning, Dynamic Strain Aging, and slip bands, are at play. The stacking fault energy (SFE) influences the percentage of mechanical twinning, which in turn affects the strain hardening rate.

MATERIALS SCIENCE AND ENGINEERING A-STRUCTURAL MATERIALS PROPERTIES MICROSTRUCTURE AND PROCESSING (2024)

Article Nanoscience & Nanotechnology

Electron beam welding of L12-nanoparticle-strengthened strong and ductile medium-entropy alloys for cryogenic applications

Hanlin Peng, Siming Huang, Ling Hu, Bingbing Luo, Liejun Li, Ian Baker

Summary: This study explores the weldability, microstructures, and mechanical properties of two L1(2)-nanoparticle-strengthened medium-entropy alloys after electron beam welding (EBW). The results show that strong yet ductile defect-free joints were produced, with larger grain sizes in the fusion zones compared to the heat-affected zones and base materials. Both EBWed MEAs exhibited high yield strengths, high ultimate tensile strengths, and good fracture strains at 77 K. The V-doping improved the cryogenic mechanical properties of the TMT MEA.

MATERIALS SCIENCE AND ENGINEERING A-STRUCTURAL MATERIALS PROPERTIES MICROSTRUCTURE AND PROCESSING (2024)

Article Nanoscience & Nanotechnology

Strain rate-dependent tensile deformation behavior and fracture mechanism of Mn-N bearing lean duplex stainless steel

Yongxin Wang, Lei Chen, Lizi Shao, Shuo Hao, Motomichi Koyama, Xingzhou Cai, Xiaocong Ma, Miao Jin

Summary: This study investigated the tensile deformation behavior of an Mn-N bearing lean duplex stainless steel with metastable austenite. The results showed that the strain rate had significant influence on the work hardening, strain-induced martensitic transformation, and fracture mechanism.

MATERIALS SCIENCE AND ENGINEERING A-STRUCTURAL MATERIALS PROPERTIES MICROSTRUCTURE AND PROCESSING (2024)

Article Nanoscience & Nanotechnology

Recovery of sheet formability of cold-rolled pure titanium by cryogenic-deformation treatment

Jong Woo Won, Seulbi Lee, Hye-Jeong Choe, Yong-Taek Hyun, Dong Won Lee, Jeong Hun Lee

Summary: Cold-rolled pure titanium showed improved sheet formability after undergoing cryogenic-deformation treatment. This treatment increased the thinning capability of the titanium and suppressed cracking during sheet forming. The formation of twins during deformation contributed to high thinning capability and increased strength through grain refinement and dislocation accumulation.

MATERIALS SCIENCE AND ENGINEERING A-STRUCTURAL MATERIALS PROPERTIES MICROSTRUCTURE AND PROCESSING (2024)

Article Nanoscience & Nanotechnology

Rapidly induced homogenization and microstructure control of Cu-15Ni-8Sn alloy by electropulsing treatment

Handong Li, Lin Su, Lijuan Wang, Yanbin Jiang, Jiahui Long, Gaoyong Lin, Zhu Xiao, Yanlin Jia, Zhou Li

Summary: Homogenization heat treatment is a key procedure in controlling the second phase, enhancing composition uniformity, and workability of as-cast Cu-15Ni-8Sn alloy. This study found that electropulsing treatment (EPT) can significantly reduce treatment temperature and time, improve elongation and overall mechanical properties of the alloy.

MATERIALS SCIENCE AND ENGINEERING A-STRUCTURAL MATERIALS PROPERTIES MICROSTRUCTURE AND PROCESSING (2024)

Article Nanoscience & Nanotechnology

Study on the regulation of microstructure and mechanical properties of Cu-15Sn-0.3Ti alloy by a novel mechanical-heat-electricity synergistic method

Yuxuan Wang, Juntao Zou, Lixing Sun, Yunfei Bai, Zhe Zhang, Junsheng Cheng, Lin Shi, Dazhuo Song, Yihui Jiang, Zhiwei Zhang

Summary: A novel mechanical-heat-electricity synergistic method was proposed to enhance the mechanical properties of Cu-15Sn-0.3Ti alloy by forming annealing twins (ATs). The combination method of Rotary swaging (RS) and Electric pulse treatment (EPT) successfully induced recrystallization and refinement of the microstructure, leading to a significant increase in the strength of the alloy within a short time.

MATERIALS SCIENCE AND ENGINEERING A-STRUCTURAL MATERIALS PROPERTIES MICROSTRUCTURE AND PROCESSING (2024)

Article Nanoscience & Nanotechnology

Ta-induced strengthening of CoCrNi-AlTi medium-entropy alloys via nanoscale heterogeneous coherent precipitate

Zhiyi Ding, Jiangtao Xie, Tong Wang, Aiying Chen, Bin Gan, Jinchao Song

Summary: This study demonstrated the Ta-induced strengthening of CoCrNi-AlTi MEAs using nanoscale heterogeneous coherent precipitates. The addition of Ta and aging treatments significantly enhanced the mechanical properties of the alloy, including yield strength, ultimate tensile strength, and elongation.

MATERIALS SCIENCE AND ENGINEERING A-STRUCTURAL MATERIALS PROPERTIES MICROSTRUCTURE AND PROCESSING (2024)

Article Nanoscience & Nanotechnology

Microstructural evolution and deformation behavior of an interstitial TRIP high-entropy alloy under dynamic loading

Z. Y. You, Z. Y. Tang, B. Wang, H. W. Zhang, P. Li, L. Zhao, F. B. Chu, H. Ding

Summary: The mechanical properties and microstructural evolution of C-doped TRIP-assisted HEA under dynamic loading conditions were systematically investigated in this study. The results showed that dynamic tensile deformation led to an increase in yield strength and a decrease in ultimate tensile strength, with a trend towards increased total elongation. The primary deformation mechanisms shifted from TRIP and TWIP effects to deformation twinning and dislocations. The presence of carbides formed through C-doping hindered dislocation slip and promoted the activation of multiple twinning systems.

MATERIALS SCIENCE AND ENGINEERING A-STRUCTURAL MATERIALS PROPERTIES MICROSTRUCTURE AND PROCESSING (2024)

Article Nanoscience & Nanotechnology

Strong resistance to shear instability in multilayered metallic composites by nanoscale amorphous-BCC crystalline interfaces

Feng Qin, Feihu Chen, Junhua Hou, Wenjun Lu, Shaohua Chen, Jianjun Li

Summary: Plastic instability in strong multilayered composites is completely suppressed by architecting nanoscale BCC Nb crystalline-amorphous CuNb interfaces.

MATERIALS SCIENCE AND ENGINEERING A-STRUCTURAL MATERIALS PROPERTIES MICROSTRUCTURE AND PROCESSING (2024)