期刊
JOURNAL OF MATERIALS SCIENCE
卷 53, 期 10, 页码 7258-7265出版社
SPRINGER
DOI: 10.1007/s10853-018-2053-6
关键词
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资金
- Science Foundation of China University of Petroleum, Beijing [2462016YJRC007, C201603]
- National Natural Science Foundation of China [21776308, 21576289]
- Science Foundation Research Funds Provided to New Recruitments of China University of Petroleum, Beijing [2462014QZDX01]
- Thousand Talents Program
Molybdenum disulfide (MoS2) has attracted a great deal of attention to its unique properties in recent years. In this work, a scalable and green method was developed for the production of high-quality MoS2 nanosheets using shear-assisted supercritical CO2 exfoliation. Our experiments indicate that high temperature, pressure, and shearing speed are favorable to the exfoliation of MoS2. It is found that over 95% of the exfoliated MoS2 nanosheets are less than 10 layers, among which about 50% are 1-4 layers. Raman spectra and XRD patterns reveal that few-layer MoS2 nanosheets with high planar crystal structure are successfully prepared. Moreover, the produced MoS2 has a better stability in N-methyl-pyrrolidone (NMP) than the bulk MoS2. The concentration of the exfoliated MoS2 in NMP after sedimentation for 7 days is as high as 0.97 mg/ml.
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