期刊
PROCESSING AND APPLICATION OF CERAMICS
卷 11, 期 3, 页码 220-224出版社
UNIV NOVI SAD, FAC TECHNOLOGY
DOI: 10.2298/PAC1703220F
关键词
zirconia; nonaqoeus synthesis; fracture; crystal structure
资金
- National Natural Science Foundation of China [51162013, 51362014]
- Major Discipline Academic and Technical Leader Training Plan Project of Jiangxi Province [20113BCB22009]
- Science and Technology Supporting Plan Project of Jiangxi Province, China [20111BBE50018]
- Science Foundation of Jiangxi Provincial Department of Education, China [GJJ150887]
- Youth Science Foundation of Jiangxi Provincial Department of Education, China [GJJ150892]
- Postdoctoral researchers preferred funded projects of Jiangxi Province [2013KY34]
- Jingdezhen Science and technology program [20161GYZD011-007]
A novel green nonaqueous sol-gel process was developed to prepare 3 mol% Y2O3-doped ZrO2 nanopowder from zirconium oxychloride and without need for washing of the obtained particles. It was shown that highly dispersive nanometer-scale zirconia powder with the particle size of 15-25 nm and BET surface area of 41.2 m(2)/g can be prepared. The sintering behaviour was also investigated. Density of the translucent body sintered at 1400 degrees C is 98.7 +/- 0.3% of its theoretical density and the surface and cross section areas are dense without holes or other defects. The bending strength of the sintered sample is 928 +/- 64 MPa.
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