期刊
RSC ADVANCES
卷 7, 期 23, 页码 13846-13850出版社
ROYAL SOC CHEMISTRY
DOI: 10.1039/c6ra26231g
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资金
- National Natural Science Foundation of China (NSFC) [51372149, 51672171, 11574194]
- National Key Basic Research Program of China [2015CB921600]
- Shanghai Municipal Education Commission
- Science and Technology Commission of Shanghai Municipality [16DZ2260600]
A single crystal of Mn4Nb2O9 of about 8 mm in diameter and 30 mm in length was successfully grown by a newly designed one-step method based on the optical floating zone technique. Clear Laue spots and sharp XRD Bragg reflections attest the good crystal quality. The antiferromagnetic phase transition at T-N = 108.4 K of the Mn4Nb2O9 single crystal was observed along the c axis, which contrasts with Co4Nb2O9 belonging to the same structural family. Structural changes with a-axis shrinkage and c-axis expansion at T-N demonstrate a significant and anisotropic magnetostriction effect.
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