期刊
CHEMICAL SCIENCE
卷 8, 期 9, 页码 6656-6661出版社
ROYAL SOC CHEMISTRY
DOI: 10.1039/c7sc02625k
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资金
- Nanyang Technological University [RG6/13, RG132/14]
- Ministry of Education, Singapore [MOE 2013-T3-1-002]
Herein, we describe an efficient method to prepare enantiomerically pure 8-oxabicyclo[3.2.1]octanes via gold(I)-catalyzed tandem 1,3-acyloxy migration/Ferrier rearrangement of glycal derived 1,6-enyne bearing propargylic carboxylates. The resultant compounds could then undergo interrupted Nazarov cyclization to afford diastereomerically pure 11-oxatricyclo[5.3.1.0]undecanes.
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