期刊
TOPICS IN CATALYSIS
卷 60, 期 9-11, 页码 782-788出版社
SPRINGER/PLENUM PUBLISHERS
DOI: 10.1007/s11244-017-0770-8
关键词
Monoclinic-tetragonal heterostructured BiVO4; Solvothermal method; EGME/water mixed solvent; Photodecomposition of Rhodamine B
资金
- Basic Science Research Program through the National Research Foundation of Korea (NRF) - Ministry of Education, Science and Technology
- National Research Foundation of Korea [2011-0006722] Funding Source: Korea Institute of Science & Technology Information (KISTI), National Science & Technology Information Service (NTIS)
A monoclinic-tetragonal heterostructure of BiVO4 was successfully synthesized by performing a solvothermal method using different molar ratio of EGME/H2O as mixed solvents. The phase structure and morphology of as-prepared BiVO4 samples were characterized by Raman spectroscopy, XRD, SEM and DRS. We have also investigated the photocatalytic activity of these materials for the decomposition of Rhodamine B under visible light irradiation. When BiVO4 was synthesized using a mixture of EGME and H2O solvents (EGME/H2O volume ratio varied from 70/10 to 10/70), XRD pattern showed the coexistence of monoclinic and tetragonal phase. From the XRD, Raman spectroscopy and SEM results, the monoclinic-tetragonal heterostructure of BiVO4 samples prepared using different volume ratios of EGME/H2O exhibited different morphologies and crystal structure. The BiVO4 catalyst, which was prepared when the volume ratio of EGME/water was set at 40/40, showed the highest photocatalytic activity in the photodegradation of Rhodamine B under visible light.
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