期刊
TETRAHEDRON
卷 73, 期 45, 页码 6443-6447出版社
PERGAMON-ELSEVIER SCIENCE LTD
DOI: 10.1016/j.tet.2017.09.041
关键词
Chiron approach; Total synthesis; Synargentolide B
资金
- National Basic Research Program of China [2015CB931903]
- National Key Research and Development Program of China [2016YFA0203102]
- Strategic Priority Research Program of Chinese Academy of Sciences [XDB14040201]
- NNSF of China [21372254, 21321004]
A concise and efficient chiron approach for the total synthesis of natural product synargentolide B was achieved in 10 steps with overall yields of 11.3% from D-mannitol and L-ethyl lactate. The key reactions included anti-Barbier allylation, cross-metathesis, and an intramolecular Yamaguchi esterification. (C) 2017 Elsevier Ltd. All rights reserved.
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