期刊
SURFACE ENGINEERING
卷 36, 期 1, 页码 69-77出版社
TAYLOR & FRANCIS LTD
DOI: 10.1080/02670844.2017.1338378
关键词
CrN; ZrN; Cr-Zr-N; wear; friction; nanoindentation
Cr-Zr-N films have been synthesised using R.F reactive magnetron sputtering system on Si (100) wafer and XC100 steel substrate without heating. The structural, mechanical and friction coefficient evolution as a function of the Zr content were investigated by XRD, (EDS, WDS), WPS, XPS, SEM, AFM, nanoindentation, Scratch adhesion and pin-on-disc sliding wear tests. The results show, that, with increasing Zr content, the film structure changed with the coexistence of (Cr-N, Zr-N) crystallographic orientation mixture. The films formed a (Cr, Zr) N solid solution where Zr atoms substitute Cr atoms. CrN lattice parameter increased from 4.17 to 4.32 angstrom with the crystallite size refinement. The mechanical parameters (H, sigma, E, H/E and H-3/E-2) were significantly improved in comparison to binary films, especially at 29 at.-% Zr. The friction and wear behaviour of the Cr-Zr (29 at.-% Zr)-N coating also showed a significant improvement.
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