期刊
JOURNAL OF THE EUROPEAN CERAMIC SOCIETY
卷 37, 期 16, 页码 5347-5351出版社
ELSEVIER SCI LTD
DOI: 10.1016/j.jeurceramsoc.2017.07.031
关键词
Spinel; MgAl2O4; Transparent ceramic; Pressureless sintering; Hot isostatic pressing
资金
- French-German Research Institute of Saint-Louis
- French Defence Procurement Agency
Transparent MgAl2O4 spinel ceramics were processed from sub-micrometric commercial powder by applying a two-step procedure: pressureless sintering under vacuum followed by hot isostatic pressing. To limit grain growth and to avoid secondary reactions or impurities, no additives or sintering aids were added to the powder. First, pressureless sintering at 1500 degrees C during 2 h under vacuum led to opaque samples due to a high level of porosity. To improve the optical quality of the MgAl2O4 ceramics and the in-line transmission in the visible range, a post-treatment by hot isostatic pressing was applied. Highly transparent ceramics were obtained after a post-treatment at 1800 degrees C for 10 h with an in-line transmission of 81% at 400 nm and 86% from 950 to 3000 nm for a thickness of 2 mm (98.8% of the theoretical transmission).
作者
我是这篇论文的作者
点击您的名字以认领此论文并将其添加到您的个人资料中。
推荐
暂无数据