4.7 Article

Iodobenzene-Catalyzed Synthesis of Phenanthridinones via Oxidative C-H Amidation

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JOURNAL OF ORGANIC CHEMISTRY
卷 82, 期 7, 页码 3589-3596

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AMER CHEMICAL SOC
DOI: 10.1021/acs.joc.7b00106

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  1. American Association for Cancer Research grant [00167155]

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We report a novel synthesis of phenanthridinones from N-methoxybenzamides using an oxidative C-H amidation reaction at room temperature in open air with modest to excellent yields. This method demonstrated unprecedented substrate scope. In particular, it solved the long-standing challenge in the synthesis of phenanthridinones with sterically demanding substitutions.

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