期刊
JOURNAL OF ORGANIC CHEMISTRY
卷 82, 期 10, 页码 5391-5397出版社
AMER CHEMICAL SOC
DOI: 10.1021/acs.joc.7b00750
关键词
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资金
- National Natural Science Foundation of China [21672104, 21502097]
- Natural Science Foundation of the Education Department of Jiangsu province [15KJB150015]
- Priority Academic Program Development of Jiangsu Higher Education Institutions
3-Cyanomethylated imidazopyridines were synthesized via a visible light-promoted reaction of imidazopyridines with bromoacetonitrile or iodoacetonitrile catalyzed by fac-Ir(ppy)(3) under mild conditions. For the substrates with various substituents on benzene or pyridine ring, the reaction proceeded smoothly to give the corresponding products in moderate to good yields. The synthetic utility of this visible light-induced reaction has been illustrated in the efficient synthesis of zolpidem and alpidem.
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