期刊
FUNCTIONAL MATERIALS LETTERS
卷 10, 期 2, 页码 -出版社
WORLD SCIENTIFIC PUBL CO PTE LTD
DOI: 10.1142/S1793604717500059
关键词
Ag2S/Ag3PO4/Ni thin film; cathodic bias; photoelectrocatalysis; rhodamine b; reaction mechanism
资金
- Science and Technology Research and Development Program of Langfang [2015011055]
Ag2S/Ag3PO4/Ni thin films were prepared using an electrochemical method. The surface morphology, phase structure, optical characteristics and band structure of the thin films were analyzed using scanning electron microscopy (SEM), X-ray diffraction (XRD) and ultraviolet-visible diffuse reflectance spectroscopy (UV-Vis DRS), respectively. Additionally, the films photoelectrocatalytic (PEC) activity and stability were evaluated using rhodamine B (RhB) as a model compound. Ag2S/Ag3PO4/Ni thin films that were prepared under optimum conditions contained nanoparticles that were approximately 25 nm in size and exhibited high PEC activity. At an optimum cathodic bias of -0.60V, the PEC degradation rate of RhB was 1.93 times greater than that of Ag3PO4/Ni thin film. Especially, the film displayed excellent PEC stability, even after being reused eight times. The possible PEC reactions between the film and RhB under visible-light irradiation are discussed in this paper.
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