期刊
EUROPEAN JOURNAL OF ORGANIC CHEMISTRY
卷 2017, 期 6, 页码 1063-1069出版社
WILEY-V C H VERLAG GMBH
DOI: 10.1002/ejoc.201601103
关键词
Multicomponent reactions; Synthetic methods; C1 building blocks; Heterocycles; Cyclization
资金
- Research Foundation - Flanders (FWO)
- Research Fund of the University of Leuven
- European Community Mobility Programme Erasmus Mundus Action 2, Strand 1
- Erasmus Mundus External Cooperation Window (EMECW) - Triple I
- Hercules Foundation [AUGE/11/029]
- Research Foundation - Flanders
- Hercules Foundation of the Flemish Government [20100225-7]
A copper-catalyzed two-step one-pot procedure for the synthesis of thiazolidine-2-thiones has been developed. The process involves a three-component coupling of an alkyne, an aldehyde, and an amine (A(3)-coupling) followed by trapping the resulting propargylamine with carbon disulfide and subsequent cyclization.
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