期刊
RSC ADVANCES
卷 6, 期 4, 页码 3198-3209出版社
ROYAL SOC CHEMISTRY
DOI: 10.1039/c5ra17110e
关键词
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资金
- UK Engineering and Physical Science Research Council (EPSRC) [EP/L017318/1]
- EPSRC [EP/L017318/1] Funding Source: UKRI
- Engineering and Physical Sciences Research Council [EP/L017318/1] Funding Source: researchfish
The crystal structure of Poly Aryl Ether Ketones (PAEKs) fabricated using a range of manufacturing processes has been investigated by high resolution electron microscopy. The study has revealed a hierarchical spherulitic crystal structure, different from the common spherulite morphology with lamellae grown in a radial direction. The results show that spherulites in laser sintered PAEKs are built of granular crystal blocks of 75-145 nm in size self-assembled along the radial direction. The study also showed that the granular crystal blocks are composed of small primary crystals approximately 20-30 nm in size combined together with a secondary structure. The secondary structure was found to be less ordered and was preferentially removed during chemical etching whereas the primary crystals remained intact.
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