期刊
CHEMISTRY-A EUROPEAN JOURNAL
卷 21, 期 9, 页码 3755-3765出版社
WILEY-V C H VERLAG GMBH
DOI: 10.1002/chem.201405659
关键词
energetic oxidisers; nitramines; structure elucidation; tetrazoles; thermal analysis
资金
- Ludwig-Maximilian University of Munich (LMU)
- U.S. Army Research Laboratory (ARL) [W911NF-09-2-0018]
- Armament Research, Development and Engineering Center (ARDEC) [W911NF-12-1-0467, W911NF-12-1-0468]
- Office of Naval Research (ONR) [ONR.N00014-10-1-0535, ONR.N00014-12-1-0538]
This combined experimental, theoretical and comparative study details the syntheses and chemical characterisation of two new energetic polynitromethyl tetrazole derivatives, namely, 2-(2-nitro-2-azapropyl)-5-(trinitromethyl)-2H-tetrazole and its fluorine-containing analogue 2-(2-nitro-2-azapropyl)-5-(fluorodinitromethyl)-2H-tetrazole. Their crystal structures and energetic behaviour are compared to those of their starting materials, the ammonium salts of the corresponding 5-(polynitromethyl)-2H-tetrazoles. Additionally, the crystal structures of two further related polynitrotetrazoles are presented.
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