期刊
ORGANIC LETTERS
卷 18, 期 14, 页码 3342-3345出版社
AMER CHEMICAL SOC
DOI: 10.1021/acs.orglett.6b01438
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资金
- Ministry of Education, Youth and Sport of the Czech Republic [IGA_PrF_2016_020]
- European Social Fund [CZ.1.07/2.3.00/20.0009]
- National Program of Sustainability [LO1304]
One-step replacement of NH2 groups in ring-substituted anilines by deuterium is reported. Approaches comprising both solid-phase and solution phase syntheses can, be used on a large variety of substrates. The method uses diazotization in a mixture of water and either dichloromethane or chloroform, which serve as a source of hydrogen. This protocol can be used as a general method for fast and easy incorporation of deuterium into an aromatic system using deuterated chloroform.
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