4.8 Article

Temperature-Dependent Double Isocyanide Insertion Reaction To Construct a Polycyclic Skeleton

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ORGANIC LETTERS
卷 18, 期 4, 页码 840-843

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AMER CHEMICAL SOC
DOI: 10.1021/acs.orglett.6b00131

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  1. National Natural Science Foundation of China [21272148, 21472121, 21272147]
  2. Key Laboratory of Synthetic Chemistry of Natural Substances, Shanghai Institute of Organic Chemistry, Chinese Academy of Science

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A novel strategy to furnish selective double insertion of isocyanides with the aid of potassium tetrachloroaurate(III) has been disclosed. This strategy provides quick access to approach a complex polycyclic skeleton in an efficient manner. Unexpected oxygen migration was also observed when the reaction was conducted at a lower temperature.

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