期刊
ORGANIC & BIOMOLECULAR CHEMISTRY
卷 14, 期 36, 页码 8486-8492出版社
ROYAL SOC CHEMISTRY
DOI: 10.1039/c6ob01522k
关键词
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资金
- Priority Academic Program Development of Jiangsu Higher Education Institutions (PAPD)
- NSFC [21302015, 21272165]
- Jiangsu Planned Projects for Postdoctoral Research Fund [1501094B]
- China Postdoctoral Science Foundation
A novel Bu4NI-catalyzed pyrazole formation reaction is well described via sequential [3 + 2] cycloaddition and oxidative dehydrogenation reactions using TBHP as the primary oxidant. In comparison with previous cases toward pyrazoles from alkenes and diazo compounds, alkenes without a pre-organized leaving group were applied in this transformation. In addition, this methodology was distinguished by its broad substrate scope, commercially available inexpensive starting materials, high atom economy and operational simplicity.
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