期刊
MICROSCOPY
卷 -, 期 -, 页码 -出版社
OXFORD UNIV PRESS
DOI: 10.1093/jmicro/dfad044
关键词
in situ observation; electrochemical reactions; liquid electrolytes; liquid-phase TEM; liquid-phase SEM; MEMS chips
类别
In this paper, we review notable points from observations of electrochemical reactions in a liquid electrolyte using liquid-phase electron microscopy. In-situ microscopic observations of electrochemical reactions are crucial for addressing various battery issues. Two methods, liquid-phase (scanning) transmission electron microscopy and liquid-phase scanning electron microscopy, are discussed and their advantages and disadvantages are summarized.
Herein, we review notable points from observations of electrochemical reactions in a liquid electrolyte by liquid-phase electron microscopy. In situ microscopic observations of electrochemical reactions are urgently required, particularly to solve various battery issues. Battery performance is evaluated by various electrochemical measurements of bulk samples. However, it is necessary to understand the physical/chemical phenomena occurring in batteries to elucidate the reaction mechanisms. Thus, in situ microscopic observation is effective for understanding the reactions that occur in batteries. Herein, we focus on two methods, of the liquid phase (scanning) transmission electron microscopy and liquid phase scanning electron microscopy, and summarize the advantages and disadvantages of both methods.
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