期刊
MONATSHEFTE FUR CHEMIE
卷 147, 期 11, 页码 1871-1881出版社
SPRINGER WIEN
DOI: 10.1007/s00706-016-1822-7
关键词
Bioinorganic chemistry; Carbonyl compounds; Metal complex; NMR spectroscopy; Structure activity relationship
资金
- University of Vienna
Four new metal complexes [Cu(ISO)(2)], [Cu(BUT)(2)] and [Zn(ISO)(2)], [Zn(BUT)(2)] of the polyhydroxychalcones (isoliquiritigenin and butein) are synthesized, structurally characterized and their antioxidant activity is investigated. The formation of the complexes [Cu(ISO)(2)] and [Zn(ISO)(2)] is followed by Job's plot using NMR titration. The resulting compounds are characterized by mass spectrometry, IR spectroscopy, and elemental analysis. Studies on the radical scavenging activity are performed using DPPH as substrate. The results showed that the antioxidant activities of isoliquiritigenin and butein are enhanced after binding to copper or zinc.
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