期刊
CHEMICAL COMMUNICATIONS
卷 51, 期 84, 页码 15410-15413出版社
ROYAL SOC CHEMISTRY
DOI: 10.1039/c5cc06293d
关键词
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资金
- Engineering and Physical Sciences Research Council [EP/L018500, EP/M013820]
- EPSRC [EP/M013820/1, EP/L018500/1] Funding Source: UKRI
- Engineering and Physical Sciences Research Council [EP/M013820/1, EP/L018500/1] Funding Source: researchfish
The PSYCHE method for pure shift NMR is exploited to generate 2D J spectra with full decoupling in one dimension and multiplet structure in the other, allowing spin-spin coupling constants to be measured even in very crowded spectra. Significant improvements over existing techniques are demonstrated for the hormones estradiol and androstenedione.
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