期刊
CHEMICAL COMMUNICATIONS
卷 51, 期 30, 页码 6489-6492出版社
ROYAL SOC CHEMISTRY
DOI: 10.1039/c4cc10397a
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资金
- U. S. NSF [CHE-1305125, CHE-1408865]
- Office of Science, Office of Basic Energy Sciences, of the U.S. Department of Energy [DE-AC02-05CH11231]
- Robert A. Welch Foundation [AH-0033]
- Advanced Light Source, Beamline 11.3.1, Lawrence Berkeley Laboratory
- Direct For Mathematical & Physical Scien [1305125] Funding Source: National Science Foundation
- Direct For Mathematical & Physical Scien
- Division Of Chemistry [1408865] Funding Source: National Science Foundation
- Division Of Chemistry [1305125] Funding Source: National Science Foundation
The reaction of the tetrakis[di(ethoxycarbonyl)methano]-C-60 (1) with Ru-3(CO)(12) afforded the first bis-parallel C-60-metal cluster complex: parallel-[Ru-3(CO)(9)](2){mu(3)-eta(2),eta(2),eta(2)-C-60[C(COOC2H5)(2)](4)}. The two triruthenium groups are found in either a parallel or a tilted orientation relative to each other, as determined by NMR. Only the parallel form was characterized by X-ray crystallography.
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