期刊
JOURNAL OF THERMAL ANALYSIS AND CALORIMETRY
卷 127, 期 3, 页码 2101-2112出版社
SPRINGER
DOI: 10.1007/s10973-016-5831-x
关键词
Hollow glass microspheres; Fe2O3; Thermoplastic polyurethane; Flame retardant
资金
- University Research and Development Projects Shandong Province [J14LA13]
- Major Special Projects of Science and Technology from Shandong Province [2015ZDZX11011]
In this paper, the hollow glass microspheres coated with Fe2O3 (HGM-Fe2O3) were synthesized and characterized by scanning electron microscopy (SEM-EDS) and X-ray photoemission spectroscopy, respectively. Then, the flame retardant and smoke suppression properties of HGM-Fe2O3 in thermoplastic polyurethane (TPU) composites have been investigated intensively using several methods, including cone calorimeter test (CCT), smoke density test (SDT), scanning electron microscopy, and thermogravimetric analysis/infrared spectrometry. The CCT results showed that HGM-Fe2O3 can greatly enhance the flame retardance of polymer matrix materials compared with TPU. For example, HGM-Fe2O3 can reduce heat release rate, total heat release, and smoke release of TPU composites in the combustion process. The SDT results showed that HGM-Fe2O3 can effectively decrease the amount of smoke production in the test. Furthermore, the TG results indicate that HGM-Fe2O3 can decrease the initial decomposition temperature, and change the structure of char residue layer.
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