Article
Materials Science, Multidisciplinary
Ce Xiao, Jean-Yves Buffiere, Jean Michel Letang, Wolfgang Ludwig
Summary: The higher lateral coherence length of beams at high brilliance synchrotron sources can improve crack detectability in Synchrotron Radiation Computed Tomography (SRCT) images, but non-planar cracks may lead to strong artifacts, making quantitative crack analysis difficult. Investigation through phase contrast tomography simulations showed that these artifacts come from Fresnel interference patterns on the detector, which can be minimized by reducing phase contrast intensity or inclining cracks with respect to the beam trajectory plane.
MATERIALS CHARACTERIZATION
(2022)
Article
Chemistry, Multidisciplinary
Parmesh Gajjar, Thai T. H. Nguyen, Jun Sun, Ioanna D. Styliari, Hrishikesh Bale, Samuel A. McDonald, Timothy L. Burnett, Benjamin Tordoff, Erik Lauridsen, Robert B. Hammond, Darragh Murnane, Philip J. Withers, Kevin J. Roberts
Summary: This study combines X-ray computed tomography and molecular modeling, with the first application of diffraction contrast tomography to organic polycrystalline materials, investigating the crystal properties and powder packing behavior of hexamine. Crystal morphology is predicted through synthonic modeling, with DCT confirming the 3D structure of crystallography on external facets, edges, and corners. Analysis reveals agglomerate structures and orientational texture in the powder bed.
Article
Engineering, Aerospace
Arulmurugan Senthilnathan, Pinar Acar
Summary: This study focuses on the multiscale modeling of grain topology in polycrystalline microstructures, taking into account the effects of microstructural uncertainties. The grain topology is quantified using shape moment invariants, and a surrogate model is developed to analyze the effects of uncertainties on the homogenized properties of the microstructures.
Article
Materials Science, Multidisciplinary
Y. El Hachi, S. Berveiller, B. Piotrowski, J. Wright, W. Ludwig, B. Malard
Summary: In this study, the superelastic behavior of a Cu-Al-Be alloy was investigated using two high-energy synchrotron techniques. The microstructure and elastic strain/stress tensors of individual grains were determined, and finite element modeling was performed to validate the experimental results, revealing significant stress heterogeneities between grains.
Article
Materials Science, Multidisciplinary
G. Garces, J. Medina, B. Chavez, P. Perez, R. Barea, A. Stark, N. Schell, P. Adeva
Summary: During aging of AZ91 alloy, precipitation of Mg17Al12 increases the yield strength of the alloy, with the magnesium matrix transferring some internal load to the harder Mg17Al12 intermetallic phase through accumulation of dislocations at the interface. At 200 degrees C, dislocations can easily shear through or climb around Mg17Al12 precipitates, reducing their reinforcing capacity and increasing the load borne by the magnesium matrix.
METALLURGICAL AND MATERIALS TRANSACTIONS A-PHYSICAL METALLURGY AND MATERIALS SCIENCE
(2021)
Article
Chemistry, Multidisciplinary
Axel Henningsson, Stephen A. Hall
Summary: This article describes and demonstrates an open source Python package called xrd_simulator, which is capable of simulating geometrical interactions between a monochromatic X-ray beam and a polycrystalline microstructure. The software uses a tetrahedral mesh representation to simulate arbitrary intragranular lattice variations of single crystals embedded within a multiphase 3D aggregate. By approximating the X-ray beam as an arbitrary convex polyhedral region in space and allowing continuous motion of the sample through rigid motions, data from standard and non-standard measurement sequences can be simulated. The software enables the numerical exploration of sample reconstruction possibilities and optimization of experimental run times and sampling.
JOURNAL OF APPLIED CRYSTALLOGRAPHY
(2023)
Article
Metallurgy & Metallurgical Engineering
G. Garces, J. Medina, P. Perez, A. Stark, N. Schell, P. Adeva
Summary: In-situ compression tests using synchrotron radiation diffraction were conducted to investigate the load partitioning between the magnesium and titanium phases in an extruded Mg-15%Ti (vol.%) composite from room temperature up to 300 degrees C. The results showed that the magnesium matrix composite deforms mainly by the activation of the extension twinning system up to 200 degrees C, and the volume fraction of twins increases with plastic strain but decreases with compression temperature. Hard titanium particles bear an additional load transferred by the soft magnesium matrix from room temperature up to 300 degrees C. Twins within magnesium grains behave as an additional reinforcement at low temperature (below 200 degrees C), inducing an increase in the work hardening of the composite.
JOURNAL OF MAGNESIUM AND ALLOYS
(2023)
Article
Materials Science, Multidisciplinary
J. Medina, P. Perez, M. F. Vega, G. Garces, E. Maawad, N. Schell, P. Adeva
Summary: A complete microstructural characterization of the stoichiometric Ni2Cr alloy after different ageing times in which different degrees of order are attained has been carried out. The study used synchrotron radiation diffraction to monitor the order-disorder transformation and found that the onset temperature is higher than previous reports. In addition, fine carbide precipitation was observed, which may contribute to the strengthening of the alloy.
MATERIALS CHARACTERIZATION
(2022)
Article
Engineering, Multidisciplinary
Francisco Mesquita, Yentl Swolfs, Stepan V. Lomov, Larissa Gorbatikh
Summary: This study conducted in-situ synchrotron computed tomography (CT) tensile tests and modeling to investigate the hybrid effect in carbon-glass hybrid composites. The results showed that hybrid composites have a higher fiber break density in their carbon plies compared to non-hybrid carbon fiber composites. Fibers near a ply interface were more likely to fail, augmenting the hybrid effect.
COMPOSITES PART B-ENGINEERING
(2022)
Article
Materials Science, Multidisciplinary
Zifan Wang, Jingwei Chen, Oxana V. Magdysyuk, Fatih Uzun, Alexander M. Korsunsky
Summary: This paper introduces a new method to extract texture information from single shot diffraction patterns and demonstrates another texture analysis method based on single shot X-ray diffraction. The effectiveness of both methods is proven through evaluation on polycrystalline nickel-based superalloy samples. Additionally, a new metric is proposed to quantify the matching quality of pole figures.
MATERIALS CHARACTERIZATION
(2022)
Article
Materials Science, Multidisciplinary
J. C. Stinville, W. Ludwig, P. G. Callahan, M. P. Echlin, V. Valle, T. M. Pollock, H. Proudhon
Summary: This study enables imaging of bulk slip events within the 3D microstructure through the combined use of X-ray diffraction contrast tomography and topotomography. Correlative measurements were performed using various methods to validate the observation of slip events and significant differences were found between bulk and surface grains, highlighting the need for 3D observations to better understand deformation in polycrystalline materials.
MATERIALS CHARACTERIZATION
(2022)
Article
Mechanics
Jesbeer Kallungal, Laurent Chazeau, Jean-Marc Chenal, Jerome Adrien, Eric Maire, Claire Barres, Bernard Cantaloube, Patrick Heuillet, Fabien Wilde, Julian Moosmann, Timm Weitkamp
Summary: This paper presents a precise 3D quantification of damage evolution and crack initiation in peroxide crosslinked EPDM filled with metallic oxide particles and filler agglomerates using synchrotron radiation X-ray Tomography. Polymer debonding is observed at the poles of metallic oxide particles during stretching, while crack always originates from carbon black agglomerates. The crack initiation process involves cavity nucleation, cavity growth, and eventual fracture of the agglomerates.
ENGINEERING FRACTURE MECHANICS
(2023)
Review
Chemistry, Physical
Iuliia Neumann, Bertold Rasche
Summary: Electrochemistry and diffraction are complementary techniques for studying solids and their surfaces. They provide information on thermodynamics, kinetics, and atomic structure. In situ diffraction allows for the discovery of metastable and transitional phases, as well as information on electrode surfaces. This review discusses the application of in situ diffraction beyond battery materials, presenting recent examples and available setups.
CURRENT OPINION IN ELECTROCHEMISTRY
(2023)
Article
Materials Science, Multidisciplinary
Yoshikazu Nakai, Shoichi Kikuchi, Daiki Shiozawa, Takumi Hase, Issei Nakazawa, Keisuke Fujita, Mie O. Kawabata, Kei Ameyama
Summary: Austenitic stainless steels with a bimodal harmonic structure, consisting of fine grain (Shell) around coarse grain (Core), were prepared using powder metallurgy and exhibited improved strength and ductility. X-ray diffraction contrast tomography was used to evaluate the grain shape and location and assess the dislocation density of the Core and Shell structures. The results showed higher dislocation density in the Shell structure compared to the Core structure, indicating localized deformation in the fine grain structure.
ADVANCED ENGINEERING MATERIALS
(2023)
Article
Materials Science, Multidisciplinary
M. Topping, F. Long, I. Cherubin, N. Nikpoor Badr, J. Cui, J. S. Park, M. R. Daymond
Summary: The behavior of radial hydrides in Zr-2.5Nb pressure tube samples at elevated temperature was studied. Two populations of hydrides, naturally oriented and reoriented, were observed in the samples during in-situ heating experiments. Reoriented hydrides completely dissolved at a relatively low temperature and only naturally oriented hydrides were observed on subsequent cooling. These findings present a potential route for ductility recovery in pressure tube materials where radial hydrides reduce fracture toughness.
JOURNAL OF NUCLEAR MATERIALS
(2022)