期刊
JOURNAL OF ORGANIC CHEMISTRY
卷 81, 期 23, 页码 11994-12000出版社
AMER CHEMICAL SOC
DOI: 10.1021/acs.joc.6b02181
关键词
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资金
- National Natural Science Foundation of China [21422205, 21272106, 21632001]
- Program for New Century Excellent Talents in University [NCET-13-0258]
- Changjiang Scholars and Innovative Research Team in University [IRT-15R28]
- 111 project
- Fundamental Research Funds for the Central Universities [lzujblcy-2016-ct02, lzujbky-2016-ct08]
A novel, efficient, and facile approach for the synthesis of structurally important pyrimidines has been successfully developed by Cu-catalyzed and 4-HO-TEMPO mediated [3 + 3] annulation of commercially available amidines with saturated ketones. This method provides a new protocol for the synthesis of pyrimidines by a cascade reaction of oxidative dehydrogenation/annulation/oxidative aromatization via direct beta-C(sp(3))-H functionalization of saturated ketones followed by annulation with amidines.
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