期刊
JOURNAL OF LABELLED COMPOUNDS & RADIOPHARMACEUTICALS
卷 59, 期 13, 页码 546-551出版社
WILEY-BLACKWELL
DOI: 10.1002/jlcr.3446
关键词
beta-agonist; internal standards; isotope labeling; synthesis
资金
- Ministry of Science and Technology, P. R. China [2015BAK45B01]
- Shanghai Zhangjiang Scientific Park [201505-PT-C101-010]
Three stable and simple synthetic routes of labeled D-9-Mabuterol, D-9-Bambuterol, and D-9-Cimbuterol were described with 98.5%, 99.7%, and 98.4% isotopic abundance and good purity. These structures and isotope-abundance were confirmed according to H-1 NMR and liquid chromatography-tandem mass spectrometry.
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