期刊
JOURNAL OF INORGANIC AND ORGANOMETALLIC POLYMERS AND MATERIALS
卷 26, 期 2, 页码 353-358出版社
SPRINGER
DOI: 10.1007/s10904-016-0327-5
关键词
Novel complex; Mixed oxide; Thermal decomposition; XRD; SEM; VSM
资金
- University of Sistan and Baluchestan (USB)
The following investigation reports the synthesis of novel complex [Fe(opd)(3)](2)[Ba(CN)(8)] and preparation of BaFe2O4 nanoparticles through thermal decomposition without using any surfactant. The complex was characterized via Furrier transform infrared spectroscopy (FT-IR), ultra violet-visible spectroscopy (UV-vis), conductivity measurement and elemental analysis. The synthesized crystals of inorganic precursor complex was transferred to furnace, where they were calcined under normal atmosphere condition at 900 A degrees C for 4 h. Formation of BaFe2O4 was supported by FT-IR and energy-dispersive X-ray analysis. Hexagonal structure of nano-oxide was confirmed on powder X-ray diffraction. Furthermore, uniform morphology of nanocrystals were reported by scanning electron microscopy. The saturation magnetization (22 emu/g), remanent magnetization (6 emu/g) and coercivity (400 Oe) reported on vibrating sample magnetometer curve illustrates the promising industrial and medicinal applications of prepared mixed oxide.
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