Electrochemical determination of paracetamol by SWCNT-modified carbon paste electrode: a cyclic voltammetric study

The central theme of this work is the synthesis of single-walled carbon nanotubes (SWCNTs) through the chemical vapor deposition method (CVD). Single-walled carbon nanotubes are synthesized using catalyst-chemical vapor deposition of acetylene at 750 degrees C temperature. X-ray diffraction study gives a characteristic peak (002) at 26.55 degrees corresponding to the existence of carbon nanotube confirms that the particles are crystalline in nature and hexagonal phase. An SEM and HR-TEM outcome gives surface morphology of SWCNTs. The elemental composition was confirmed by EDAX. The ideal concentration of single-walled carbon nanotubes was used to design a novel electrochemical sensor for determining paracetamol (PA) using cyclic voltammetry. Electrochemical determination of paracetamol is described using a single-walled carbon nanotube modified carbon paste electrode (SWCNT/MCPE). The SWCNT/MCPE was used in this study to detect paracetamol electrochemically at pH 7.2 in a 0.2 M PBS with a scan rate of 50 mV s(-1). A single-walled nanotube modified carbon paste electrode was used to develop a sensitive and selective electrochemical technique for the detection of PA. The SWCNT/MCPE showed excellent electrocatalytic activity towards the oxidation of paracetamol in phosphate buffer solution. Therefore, with increased oxidation currents, the voltammetric responses of paracetamol at the bare carbon paste electrode are organized within cyclic voltammetric peaks. [GRAPHICS] .

Automated summary

The central theme of this work is the synthesis of single-walled carbon nanotubes using the chemical vapor deposition method. The synthesized nanotubes were characterized using X-ray diffraction, SEM, HR-TEM, and EDAX. A novel electrochemical sensor was designed using the single-walled carbon nanotubes, and it showed excellent electrocatalytic activity for the detection of paracetamol.