4.2 Article

The lower energy diffraction and scattering side-bounce bean dine for materials science a the Canadian Light Source

期刊

JOURNAL OF SYNCHROTRON RADIATION
卷 28, 期 -, 页码 961-969

出版社

INT UNION CRYSTALLOGRAPHY
DOI: 10.1107/S1600577521002496

关键词

hard X-ray diffraction; X-ray scattering; in-vacuum wiggler; side-bounce monochromator; powder diffraction

资金

  1. Canada Foundation for Innovation (CFI)
  2. Natural Sciences and Engineering Research Council (NSERC)
  3. National Research Council (NRC)
  4. Canadian Institutes of Health Research (CIHR)
  5. Government of Saskatchewan
  6. University of Saskatchewan

向作者/读者索取更多资源

A new diffraction beamline for materials science has been constructed at the Canadian Light Source synchrotron, offering various techniques for materials research such as high-resolution powder diffraction and small molecule crystallography. The beamline features a vertical x horizontal focused beam with a wide photon energy range and high photon flux.
A new diffraction beamline for materials science has been built at the Canadian Light Source synchrotron. The X-ray source is an in-vacuum wiggler with a 2.5 T peak magnetic field at 5.2 mm gap. The optical configuration includes a toroidal mirror, a single side-bounce Bragg monochromator, and a cylindrical mirror, producing a sub-150 ium vertical x 500 ium horizontal focused beam with a photon energy range of 7-22 keV and a flux of 10(12) photons per second at the sample position. Three endstations are currently open to general users, and the techniques available include high-resolution powder diffraction, small molecule crystallography, X-ray reflectivity, in situ rapid thermal annealing, and SAXS/ WAXS. The beamline design parameters, calculated and measured performance, and initial experimental results are presented to demonstrate the capabilities for materials science.

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