4.6 Article

Investigation of Internal Cracks in Epoxy-Alumina Using In Situ Mechanical Testing Coupled with Micro-CT

期刊

JOM
卷 73, 期 8, 页码 2452-2459

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SPRINGER
DOI: 10.1007/s11837-021-04714-x

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资金

  1. National Science Foundation [1826221]
  2. Div Of Civil, Mechanical, & Manufact Inn
  3. Directorate For Engineering [1826221] Funding Source: National Science Foundation

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Polymer-ceramic composites, such as epoxy-alumina, are commonly used in biomedical applications. Experimental investigation on crack extension in epoxy-alumina revealed that fracture toughness decreased with increasing filler fraction. The weakest link in the material was found to be the matrix-particle interfaces, where cracks often initiated from, and crack bridging by uncracked ligament and crack deflection were observed as common toughening mechanisms. Increasing matrix-particle interface strength is recommended for designing more robust epoxy-alumina composites in future work.
Polymer-ceramic composites are widely used in biomedical applications. This paper presents the results of an experimental investigation on the crack extension inside epoxy-alumina. Specimens with 5 vol.%, 10 vol.%, horizontal ellipsis , 25 vol.% fillers fractions were fabricated. Three-point bending on single-edge notched bend specimens were performed using conventional mechanical tester and in situ mechanical tester coupled with micro-CT, respectively. Fracture toughness was measured to be 2.10-2.51 MPa root m, and it decreased with increasing filler fraction. When cracks were shorter than 0.88 mm, crack resistance for 5 and 25 vol.% epoxy-alumina was similar. Beyond 0.88 mm, 25 vol.% epoxy-alumina exhibited no crack resistance, whereas stress intensity factor kept increasing in 5 vol.% epoxy-alumina. The matrix-particle interfaces were the weakest link, where cracks often initiated from. Crack bridging by uncracked ligament and crack deflection were commonly observed toughening mechanisms. To design robust epoxy-alumina composites, increasing matrix-particle interface strength is recommended for future work.

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