期刊
JOURNAL OF ORGANIC CHEMISTRY
卷 86, 期 22, 页码 15897-15905出版社
AMER CHEMICAL SOC
DOI: 10.1021/acs.joc.0c03026
关键词
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资金
- National Natural Science Foundation of China [21672104, 21502097]
- Priority Academic Program Development of Jiangsu Higher Education Institutions
An electrochemical oxidative regioselective C-H cyanation of imidazo[1,2-a]pyridines was developed utilizing TMSCN as the cyano source, with the KH2PO4/K2HPO4 buffer being essential for the transformation. This protocol was compatible with a broad range of substituted imidazo[1,2-a]pyridines and provided the C3 cyanated products in moderate to excellent yields.
Electrochemical oxidative regioselective C-H cyanation of imidazo[1,2-a]pyridines was developed using readily available TMSCN as the cyano source. The KH2PO4/K2HPO4 buffer was essential for this transformation. This protocol was compatible with a broad range of substituted imidazo[1,2-a]pyridines and provided the C3 cyanated products in moderate to excellent yields.
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