期刊
CHEMICAL COMMUNICATIONS
卷 52, 期 98, 页码 14169-14172出版社
ROYAL SOC CHEMISTRY
DOI: 10.1039/c6cc07756k
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资金
- EPSRC [EP/K504555/1]
- QinetiQ [EP/K504555/1]
The phase changes that occur during lithium extraction from LiCoPO4 in lithium half-cells were studied using synchrotron X-ray diffraction. The existence of two two-phase regions with an intermediate phase present was observed. Significant variations in the composition of the phases of nominal stoichiometry LiCoPO4, Li2/3CoPO4 and CoPO4 resulted in unit cell volume variations. On current pulsing, lattice parameter shifts and phase recovery were directly observed.
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