期刊
SCRIPTA MATERIALIA
卷 178, 期 -, 页码 39-43出版社
PERGAMON-ELSEVIER SCIENCE LTD
DOI: 10.1016/j.scriptamat.2019.11.010
关键词
Cold-rolled pure Ti; Electropolishing; FCC phase; Scanning transmission electron microscopy (STEM); Electron energy loss spectroscopy (EELS); Atom probe tomography (APT)
类别
资金
- China Scholarship Council (CSC)
- [ERC-CoG-SHINE-771602]
A face-centered cubic (FCC) phase in electro-polished specimens for transmission electron microscopy of commercially pure titanium has sometimes been reported. Here, a combination of atom-probe tomography, scanning transmission electron microscopy and low-loss electron energy loss spectroscopy is employed to study both the crystal structural and chemical composition of this FCC phase. Our results prove that the FCC phase is actually a TiHx (x >= 1) hydride, and not a new allotrope of Ti, in agreement with previous reports. The formation of the hydride is discussed. (C) 2019 Acta Materialia Inc. Published by Elsevier Ltd. All rights reserved.
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