4.7 Article

Physical, mechanical, thermal and structural characteristics of nanoencapsulated vitamin E loaded carboxymethyl cellulose films

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PROGRESS IN ORGANIC COATINGS
卷 138, 期 -, 页码 -

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ELSEVIER SCIENCE SA
DOI: 10.1016/j.porgcoat.2019.105383

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Nanoencapsulation; alpha-tocopherol; Carboxymethyl cellulose film; FTIR

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Nanoencapsulated vitamin E (alpha-tocopherol) incorporated into the carboxymethyl cellulose (CMC) films using film-forming cast solution method. Then, some physical, mechanical, thermal and structural attributes of the active films were scrutinized. From the obtained results, addition of a-tocopherol nanocapsules significantly (p < 0.05) decreased the water vapour permeability (WVP), tensile strength (TS) and Young's modulus, while elongation at break (EAB) significantly (p < 0.05) increased. Morphology of CMC films revealed that nano-capsules cause porosity and changes in film matrix structure. The DSC (differential scanning calorimetry) patterns exhibited a drop in melting points of the film composites as a result of a-tocopherol addition. The FTIR (Fourier transform infrared spectroscopy) spectra confirmed the successful loading of alpha-tocopherol into the structure of CMC films, due to the formation of carbonyl group (C=O) via phenol part of a-tocopherol at 1710 cm(-1) within the CMC film. a-tocopherol loaded CMC composite films could be proposed for sheltering food items containing lipids or fats which stored at the ambient temperature.

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