4.5 Article

Critical examination of experimental data on strain bursts (pop-in) during spherical indentation

期刊

JOURNAL OF MATERIALS RESEARCH
卷 35, 期 8, 页码 1028-1036

出版社

CAMBRIDGE UNIV PRESS
DOI: 10.1557/jmr.2019.416

关键词

nanoindentation; simulation; strength

向作者/读者索取更多资源

Pop-in during indentation testing is a term used to indicate the sudden displacement burst during loading. Experimental data are measured during an indentation pop-in event, using displacement sensors with 20 mu s time constant at 100 kHz data acquisition rate. The load-depth response during the pop-in event that occurs within 160 mu s is determined after accounting for the instruments' dynamic response. Unlike the response reported in the literature for force-controlled tests, wherein the load on the sample remains constant during the pop-in, a steep load drop is observed after the onset of pop-in, followed by a significant increase in the load well beyond the load at the onset of pop-in. A model for the material and instrument's dynamic response is presented that agrees well with the experimental observations. The implications of these findings for determination of pop-in length or velocity and for performing displacement-controlled testing involving closed loop control are discussed.

作者

我是这篇论文的作者
点击您的名字以认领此论文并将其添加到您的个人资料中。

评论

主要评分

4.5
评分不足

次要评分

新颖性
-
重要性
-
科学严谨性
-
评价这篇论文

推荐

Article Materials Science, Composites

A nanoindentation based study to evaluate the effect of carbon nanofibers on the mechanical properties of SiC composites

Shaik Mubina, P. Sudharshan Phani, Asit Kumar Khanra, Bhaskar Prasad Saha

Summary: An advanced high-speed nanoindentation technique was employed to analyze the combined reinforcing effect of carbon fibers in the SiC matrix. Various types of composite tubes were produced by introducing different forms of carbon fibers and composite powders, and the properties of the tubes were evaluated using traditional processes as well as nanoindentation techniques.

COMPOSITE INTERFACES (2021)

Article Materials Science, Multidisciplinary

Influence of Ti and Zr alloying elements on microstructure and micromechanical properties of near-eutectic Nb-18.7Si alloy

Geethasree Kommineni, Alam Md Zafir, P. Sudarshan Phani, Rajdeep Sarkar, V. V. Satya Prasad, Brahma Raju Golla

Summary: The addition of Ti and Zr alloying elements resulted in the formation of equilibrium alpha-Nb5Si3 phase in situ, improving the properties of the alloys and being cost effective. The volume fraction of the Nb-ss phase increased with the addition of elements, with hardness increasing with Ti and decreasing with Zr.

MATERIALS CHARACTERIZATION (2021)

Article Materials Science, Multidisciplinary

A novel nanoindentation protocol to characterize surface free energy of superhydrophobic nanopatterned materials

E. M. Rossi, P. Sudharshan Phani, R. Guillemet, Julie Cholet, Doriane Jussey, W. C. Oliver, M. Sebastiani

Summary: The novel nanoindentation based method presented in this work is able to measure the pull-off adhesive forces covering hydrophilic to super-hydrophobic surfaces, with potential applications in fast non-destructive mapping of SFE over heterogeneous surfaces. The method's limitations and shortcomings in reliability and reproducibility of results are critically discussed, focusing on experimental issues that could affect the measurements.

JOURNAL OF MATERIALS RESEARCH (2021)

Article Materials Science, Multidisciplinary

Measurement of hardness and elastic modulus by load and depth sensing indentation: Improvements to the technique based on continuous stiffness measurement

P. Sudharshan Phani, W. C. Oliver, G. M. Pharr

Summary: The method for measuring hardness and elastic modulus of small volumes of material through instrumented indentation was initially developed by Oliver and Pharr in their early works. This has led to advancements in the field of small scale nanomechanical testing, with improvements in measurement electronics allowing testing under a wider range of conditions. The article provides an updated overview of factors affecting precision and accuracy of nanoindentation test results, focusing on the continuous stiffness measurement technique (CSM) and presenting a step-by-step procedure for conducting CSM based tests, along with calibration procedures for optimal precision and accuracy. Additionally, an assessment and comparison of different testing procedures is presented.

JOURNAL OF MATERIALS RESEARCH (2021)

Article Nanoscience & Nanotechnology

New insights on recovery and early recrystallization of ferrite-pearlite banded cold rolled high strength steels by high speed nano-indentation mapping

S. Janakiram, P. Sudharshan Phani, Govind Ummethala, Sairam K. Malladi, J. Gautam, Leo A. Kestens

Summary: This study investigates the structure-property correlations at the micrometer length scale during recovery and early recrystallization of a cold rolled high strength steel composed of ferrite and pearlite. High resolution nano-indention mapping technique and electron microscopy were used to study the local microstructure and hardness variations with annealing temperature. A clustering algorithm was employed to determine the properties of the constituent microstructural features.

SCRIPTA MATERIALIA (2021)

Article Materials Science, Multidisciplinary

Length-scale-dependent stress relief mechanisms in indium at high homologous temperatures

Fereshteh Mallakpour, Masoud Kasraie, Erik G. Herbert, P. Sudharshan Phani, Stephen A. Hackney

Summary: Nanoindentation and electron microscopy were used to study the length-scale-dependent stress relaxation mechanisms in well-annealed, high-purity indium. The experiments identified two distinct surface morphologies of residual hardness impressions, indicating different deformation mechanisms. The formation and growth of metallic dendrites were explained by the stress relaxation mechanisms at the buried interface between metallic anode and solid electrolyte separator.

JOURNAL OF MATERIALS RESEARCH (2021)

Article Materials Science, Multidisciplinary

On the effective load during nanoindentation creep testing with continuous stiffness measurement (CSM)

P. Sudharshan Phani, W. C. Oliver, G. M. Pharr

Summary: Accurately determining the applied load is crucial in measuring hardness, especially in nanoindentation testing with continuous stiffness measurement (CSM). This study proposes the concept of an effective load during nanoindentation creep testing with CSM and validates it through theoretical analysis and experiments, finding significant implications for rate-dependent materials.

JOURNAL OF MATERIALS RESEARCH (2021)

Article Nanoscience & Nanotechnology

On the origins of ultra-high hardness and strain gradient plasticity in multi-phase nanocrystalline MoNbTaTiW based refractory high-entropy alloy

Deekshith G. Kalali, Sairam Antharam, Mohsin Hasan, P. Sai Karthik, P. Sudharshan Phani, K. Bhanu Sankara Rao, Koteswararao Rajulapati

Summary: The remarkably high hardness in the alloy, achieved through careful microstructural engineering and optimal addition of alloying elements, suggests potential for developing novel structural materials based on a multi-principal element approach.

MATERIALS SCIENCE AND ENGINEERING A-STRUCTURAL MATERIALS PROPERTIES MICROSTRUCTURE AND PROCESSING (2021)

Article Nanoscience & Nanotechnology

Role of stacking fault energy (SFE) on the high strain rate deformation of cold sprayed Cu and Cu?Al alloy coatings

Naveen Manhar Chavan, P. Sudharshan Phani, M. Ramakrishna, L. Venkatesh, Prita Pant, G. Sundararajan

Summary: Cold spray deposition involves unique combination of high strain rate and moderate to high strain deformation, leading to significant grain refinement and deformation twinning in Cu and Cu-Al alloys. Experimental observations align well with theoretical predictions, showing significant heterogeneity in cold spray coatings and identifying factors influencing hardness. Twin mediated deformation mechanism is found to explain the lower boundary strengthening in presence of fine twins.

MATERIALS SCIENCE AND ENGINEERING A-STRUCTURAL MATERIALS PROPERTIES MICROSTRUCTURE AND PROCESSING (2021)

Article Materials Science, Multidisciplinary

Rigorous analysis and pragmatic guidelines in estimating strain rate sensitivity using stress relaxation test

Kali Prasad, Vikram Balaji, Hariharan Krishnaswamy, P. Sudharshan Phani, Pierpaolo Carlone

Summary: This study demonstrates that the value of strain rate sensitivity estimated from stress relaxation tests is inaccurate and proposes a new method for accurately determining this value.

MECHANICS OF MATERIALS (2022)

Article Materials Science, Multidisciplinary

On the measurement of hardness at high strain rates by nanoindentation impact testing

P. Sudharshan Phani, B. L. Hackett, C. C. Walker, W. C. Oliver, G. M. Pharr

Summary: This study proposes an analytical framework to guide high strain rate hardness measurements through nanoindentation testing. The research results demonstrate the wide potential applications of nanomechanical measurements with low noise, fast time constants, and high data acquisition rates.

JOURNAL OF THE MECHANICS AND PHYSICS OF SOLIDS (2023)

Article Physics, Applied

Synthesis and characterization of metal carbides for nanoindentation tip applications

L. A. Boatner, C. B. Finch, W. E. Brundage, J. A. Kolopus, G. R. Gruzalski, K. E. Johanns, P. Sudharshan Phani, G. M. Pharr, W. C. Oliver

Summary: Instrumented indentation experiments at elevated temperatures require careful attention to experimental details, including the choice of indenter tip material. This study used rf-induction heating float-zone and high-temperature solution single-crystal growth techniques to prepare a suite of bulk refractory carbide specimens. These materials were characterized and compared to sapphire and polycrystalline WC-Co, and the results showed that single-crystal WC is a promising candidate for elevated-temperature nanoindentation tips.

JOURNAL OF APPLIED PHYSICS (2023)

Article Materials Science, Multidisciplinary

A unified approach to quantify the material and geometrical effects in indentation size effect

Harita Seekala, Lavakumar Bathini, Nitin P. P. Wasekar, Hariharan Krishnaswamy, P. Sudharshan Phani

Summary: The seminal work of Nix and Gao laid the foundation for quantifying the indentation size effect (ISE). This study presents a unified approach to quantify ISE by considering the effects of materials, geometry, and other coupled parameters. Experimental studies on pulsed electro-deposited nickel validate the model predictions for the depth dependence of hardness. Factors such as grain size, dislocation density, tip geometry, constraint factors, and plastic zone size are found to affect ISE.

JOURNAL OF MATERIALS RESEARCH (2023)

Article Nanoscience & Nanotechnology

Influence of additives induced microstructural parameters on mechanical behavior of (111)-oriented nanotwinned microcrystalline copper

Chetan Singh, Hariharan Krishnaswamy, Sudarshan Phani Pardhasaradhi, Fu Chian Chen, Dinh-Phuc Tran, Chih Chen, Jayant Jain

Summary: Depth sensing nanoindentation experiments were conducted to investigate the strain rate dependentindependent behaviors of nanotwinned microcrystalline Cu. Different additives were used for electro-deposition to control microstructural parameters, such as grain size and twin spacing. The sample with the lowest twin lamella spacing exhibited a lower stress exponent, potentially leading to enhanced ductility. The mechanical properties obtained by introducing nanotwins in coarser initial grain size are comparable to nanotwinned nanocrystalline materials, suggesting a new paradigm for a broader range of nanotwinned materials.

MATERIALS SCIENCE AND ENGINEERING A-STRUCTURAL MATERIALS PROPERTIES MICROSTRUCTURE AND PROCESSING (2023)

Article Engineering, Mechanical

Inception of macroscopic shear bands during hot working of aluminum alloys

Aditya Prakash, Tawqeer Nasir Tak, Namit N. Pai, Harita Seekala, S. V. S. Narayana Murty, P. S. Phani, Sivasambu Mahesh, P. J. Guruprasad, Indradev Samajdar

Summary: Macroscopic shear bands (MSB) may form during hot working of metallic materials. The microstructural transitions between the onset of flow instability and MSB inception are not fully understood. In this study, aluminum alloy specimens were tested at different temperatures and it was found that MSB only appeared at a certain level of deformation. The formation of MSB was explained by the development of clusters of severely deforming grains and the differential dynamic recovery between hard- and soft-oriented grains.

INTERNATIONAL JOURNAL OF PLASTICITY (2023)

暂无数据