期刊
APPLIED CLAY SCIENCE
卷 187, 期 -, 页码 -出版社
ELSEVIER
DOI: 10.1016/j.clay.2020.105489
关键词
LAPONITE (R); Covalent modification; Triazole moieties; Hydrogel
资金
- University of Palermo
- PON AIM: Attrazione e Mobilita Internazionale project [1808223-2]
LAPONITE (R) (Lap) clay mineral was successful functionalized by triazole groups in a two steps procedure. First, the Lap edges were modified with 3-azidopropyltrimethoxysilane by traditional heating and microwave irradiation. Microwave irradiation allowed us to obtain high loading onto the Lap edges in lower times compared to those obtained through conventional method. Afterwards, the triazole moieties were obtained by reaction between azido functionalized Lap and propargyl alcohol. The successful functionalization of Lap was proved by thermogravimetric analysis, FT-IR spectroscopy, dynamic light scattering and.-potential measurements. Finally, the effects of the surface modification on the gel formation ability of Lap were studied by gelation tests and the morphology of the gel phases was investigated by polarized optical microscopy measurements and diffusion experiments.
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