期刊
DOKLADY CHEMISTRY
卷 484, 期 -, 页码 1-4出版社
MAIK NAUKA/INTERPERIODICA/SPRINGER
DOI: 10.1134/S0012500819010026
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资金
- Russian Science Foundation [14-13-01115]
- Russian Science Foundation [14-13-01115] Funding Source: Russian Science Foundation
The method of synthesis of nanoscaled sodium dodecahydro-closo-dodecaborate Na-2[B12H12] is presented. The desired product has been prepared by heating to 200 degrees C the composite formed by the introduction of the triethylammonium salt [Et3NH](2)[B12H12] into the silicate matrix of sodium liquid glass. The morphology and phase composition of the synthesized sample have been studied by SEM and X-ray diffraction methods in comparison with regular Na-2[B12H12] salt. According to the obtained data, the sample under study is an amorphous composite, on the surface of which nanoscale crystals of Na-2[B12H12] are formed.
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