期刊
TETRAHEDRON LETTERS
卷 60, 期 3, 页码 248-251出版社
PERGAMON-ELSEVIER SCIENCE LTD
DOI: 10.1016/j.tetlet.2018.12.025
关键词
2-Aminobenzamide; Nitrogen heterocycle; 1,2,3-Benzotriazin-4-one; Sodium nitrite; Iodine
资金
- Council of Scientific and Industrial Research, New Delhi [BSC-0114]
An efficient transformation of 2-aminobenzamides to 1,2,3-benzotriazin-4(3H)-ones in the presence of sodium nitrite (NaNO2) and Iodine (I-2) is described. The reaction is proposed to proceed via formation of nitrosyl halide that induces nitrosylation of the amino group of 2-aminobenzamide leading to diazotization followed by intramolecular cyclization. (C) 2018 Elsevier Ltd. All rights reserved.
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