期刊
ACTA MATERIALIA
卷 105, 期 -, 页码 189-198出版社
PERGAMON-ELSEVIER SCIENCE LTD
DOI: 10.1016/j.actamat.2015.12.016
关键词
Ceramics; Residual stress; Tomography; X-ray synchrotron radiation; Environmental barrier coating (EBC)
资金
- DOE Office of Science by Argonne National Laboratory [DE-AC02-06CH11357]
- MRSEC program of the National Science Foundation at the Materials Research Center of Northwestern University [DMR-1121262]
- Northwestern University Terminal Year Fellowship
The interaction of calcium-magnesium-aluminosilicates (CMAS) with Yb2Si2O7-based multilayer environmental barrier coatings was studied using a combination of high-energy synchrotron X-ray techniques. Changes in the phase-specific stresses and lattice spacings as a function of temperature were investigated with wide-angle X-ray scattering. Small-angle X-ray scattering was used to study the interaction of CMAS with nanoporosity, while X-ray computed tomography was used to study the formation of cracks in the coating. It was found that CMAS interacts strongly with the Yb2Si2O7 topcoat, leading to changes in lattice spacing, alterations of the ambient temperature stresses, and large cracks in the CMAS that extend through the topcoat. (C) 2015 Acta Materialia Inc. Published by Elsevier Ltd. All rights reserved.
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