期刊
JOURNAL OF ORGANIC CHEMISTRY
卷 83, 期 24, 页码 15406-15414出版社
AMER CHEMICAL SOC
DOI: 10.1021/acs.joc.8b02666
关键词
-
资金
- SERB, India [ECR/2015/000600]
- DST [DST/2017/IF170766]
Herein, nickel-catalyzed sustainable strategy for the synthesis of N-substituted pyrroles using butene-1,4-diols and butyne-1,4-diols with a series of aryl-, alkyl-, and heteroarylamines is reported. The catalytic protocol is tolerant of free alcohol, halide, alkyl, alkoxy, oxygen heterocycles, activated benzyl, and the pyridine moiety and resulted in up to 90% yield. Initial mechanistic studies involving defined nickel catalyst, determination of rate, and order of reaction including deuterium-labeling experiments were performed for pyrrole synthesis.
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