期刊
APPLIED NANOSCIENCE
卷 2, 期 4, 页码 445-456出版社
SPRINGER HEIDELBERG
DOI: 10.1007/s13204-012-0058-z
关键词
Nanoindentation; Si-29 MAS NMR; Cement; Microstructural phases
资金
- King Abdulaziz City for Science and Technology (KACST) through the Science and Technology Unit at King Fahd University of Petroleum and Minerals (KFUPM) as part of the National Science, Technology and Innovation Plan [09-NAN754-04]
- National Science Foundation (NSF) award [1131369]
- Directorate For Engineering
- Div Of Chem, Bioeng, Env, & Transp Sys [0960256] Funding Source: National Science Foundation
- Directorate For Engineering
- Div Of Civil, Mechanical, & Manufact Inn [1131369] Funding Source: National Science Foundation
Microstructural composition of the hardened cement pastes are analyzed using nanoindentation and Si-29 MAS NMR after curing time periods of 7 and 28 days. Two curing conditions, room condition (20 degrees C with 0.1 MPa pressure) and an elevated condition (80 degrees C with 10 MPa pressure) are prepared to hydrate cement pastes [water to cement (w/c) ratio of 0.45]. The degree of hydration of the cement paste quantified using nanoindentation was compared with that from Si-29 MAS NMR. From nanoindentation of the hardened cement pastes, microstructural hydration products are characterized with respect to the corresponding modulus of elasticity. A hydration product, which has a relatively high modulus of elasticity over other known hydration products, was found in the hardened cement paste cured in elevated temperature and pressure. The effect of high pressure on the composition of the hydration product is discussed and it is hypothesized that the packing density of calcium-silicatc-hydratc (C-S-H) might increase when a cement paste is hydrated under high temperature and pressure.
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