期刊
JOURNAL OF MATERIALS CHEMISTRY A
卷 2, 期 41, 页码 17530-17535出版社
ROYAL SOC CHEMISTRY
DOI: 10.1039/c4ta02966f
关键词
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资金
- National Natural Science Foundation of China [51001052]
- Natural Science Foundation of Guangdong Province [S2013010015681]
- High-level Talent Project of the University in Guangdong Province
Currently, controlled synthesis of well-defined micro/nano-scaled catalysts with high performance is one of the most important subjects in the field of catalysis. In this work, single crystal Fe3O4 sub-microcubes with soft-magnetic properties were prepared by a facile and low-cost chemical reduction route, in which no capping agents, such as surfactant, polymer stabilizer or complexant is used. It has been demonstrated that the as-prepared Fe3O4 sub-microcubes exhibited high catalytic activity in the reduction of p-nitrophenol to p-aminophenol with hydrazine hydrate. The activation energy of the reaction is 28.9 kJ mol(-1), which is significantly lower than that of many nanocatalysts recently reported in literature. The recyclable Fe3O4 sub-microcubes can be easily separated from the reaction system by an external magnet and they do not lose their catalytic activity after 6 cycles, thus demonstrating their good reusability.
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