期刊
RSC ADVANCES
卷 3, 期 44, 页码 21964-21971出版社
ROYAL SOC CHEMISTRY
DOI: 10.1039/c3ra42818d
关键词
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资金
- US Department of Energy, the Office of Science [DE-SC0006930]
- DOE Great Lakes Bioenergy Research Center (DOE Office of Science BER) [DE-FC02-07ER64494]
- U.S. Department of Energy (DOE) [DE-SC0006930] Funding Source: U.S. Department of Energy (DOE)
We report here a reliable and facile synthesis of a range of monolignol gamma-p-hydroxycinnamate (including p-coumarate, ferulate, and caffeate), gamma-acetate, and gamma-p-hydroxybenzoate conjugates, many not previously reported, that are either putative intermediates in the biosynthesis of natural lignins or new monomer-conjugates destined for upcoming designer lignins. The key was the development of a highly selective deacylation approach for phenolic acetates; i.e., a method that cleaves phenolic acetates while leaving the sensitive monolignol ester conjugates intact.
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