期刊
ACS CATALYSIS
卷 8, 期 10, 页码 9537-9542出版社
AMER CHEMICAL SOC
DOI: 10.1021/acscatal.8b02928
关键词
copper catalysis; decarboxylative borylation; redox-active esters; practical protocol; kinetic studies
资金
- NIH [GM-118176]
- Swedish Research Council
- Foundation Blanceflor Boncompagni-Ludovisi nee Bildt
- Stiftelsen Olle Engkvist Byggmastare
- Werthen Fund Scholarship
- Zhejiang Yuanhong Medicine Technology Co. Ltd.
- Sao Paulo Research Foundation (FAPESP) [2017/08128-7]
- NATIONAL INSTITUTE OF GENERAL MEDICAL SCIENCES [R35GM118176] Funding Source: NIH RePORTER
A simple method for the conversion of carboxylic acids to boronic esters via redox-active esters (RAEs) is reported using copper catalysis. The scope of this transformation is broad, and compared with the known protocols available, it represents the most inexpensive, rapid, and operationally simple option. In addition to a full exploration of the scope, a kinetic study was performed to elucidate substrate and reagent concentration dependences.
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