期刊
ULTRASONICS SONOCHEMISTRY
卷 17, 期 1, 页码 159-161出版社
ELSEVIER SCIENCE BV
DOI: 10.1016/j.ultsonch.2009.06.012
关键词
Malononitrile; Pyrazolophthalazine; Phthalhydrazide; Ultrasound
Triethylamine was found to be an efficient catalyst for the synthesis of 1H-pyrazolo[1,2-b]phthalazine-5,10-diones by one-pot reaction of phthalhydrazide, aromatic aldehydes, and malononitrile or ethyl cyanoacetate in ethanol under ultrasonic irradiation. The advantages of this method are the use of an inexpensive and readily available catalyst, easy workup, improved yields, and the use of ethanol as a solvent that is considered to be relatively environmentally benign. (C) 2009 Elsevier B.V. All rights reserved.
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