Article
Chemistry, Analytical
Hui-Min Zhai, Bin Ji, Shan-Shan Tian, Fang Fang, Shuang Zhao, Zhi-Yong Wu
Summary: This study introduces a new method for Cr speciation analysis based on a paper-based analytical device (PAD), which uses electrokinetic separation and stacking to separate and recover Cr (VI) and Cr (III) with high sensitivity and recovery rates. This fast, cheap, and easy-to-use sample pretreatment method can be applied for direct analysis of Cr (VI)/Cr (III) in electroplating wastewater samples.
Article
Environmental Sciences
Yajie Tian, Jianzheng Li, Xianhui Li, Jiuling Li, Jia Meng
Summary: The developed method for simultaneous extraction and determination of eight veterinary antibiotics in swine wastewater and activated sludge showed good recoveries, low deviations, and high sensitivity. It has been successfully applied to evaluate the actual concentration levels of antibiotics in the two complex environmental matrices.
ENVIRONMENTAL SCIENCE AND POLLUTION RESEARCH
(2022)
Article
Chemistry, Multidisciplinary
Vasileios Alampanos, Victoria Samanidou
Summary: The sample preparation workflow of any biological sample is crucial in analytical methodology, with green analytical chemistry driving the development of new techniques and materials in bioanalysis. This has led to the establishment of novel green approaches in the field.
CURRENT OPINION IN GREEN AND SUSTAINABLE CHEMISTRY
(2021)
Review
Chemistry, Analytical
Antonio Martin-Esteban
Summary: The use of molecularly imprinted polymers in sample preparation as selective sorbent materials has gained significant attention in recent years, leading to analytical methods with unprecedented selectivity. However, with the increasing adoption of Green Analytical Chemistry principles, it is important to critically review the greenness of synthesis and further application of molecularly imprinted polymers. This review discusses the preparation steps and strategies, reagents used, as well as their incorporation into microextraction techniques from a green perspective, and offers recent alternatives to enhance the sustainability of molecularly imprinted polymers.
JOURNAL OF SEPARATION SCIENCE
(2022)
Review
Chemistry, Analytical
Alvaro Santana-Mayor, Ruth Rodriguez-Ramos, Antonio Herrera-Herrera, Barbara Socas-Rodriguez, Miguel Angel Rodriguez-Delgado
Summary: The development of sustainable chemistry has led to the emergence of new materials, with deep eutectic solvents (DESs) as a promising non-toxic alternative to toxic organic solvents, seeing a significant increase in their applications in analytical chemistry in recent years. The vast amount of information generated from studies associated with DESs needs continuous revision.
TRAC-TRENDS IN ANALYTICAL CHEMISTRY
(2021)
Review
Chemistry, Analytical
Seyedeh Sara Nasrollahi, Negar Sabahi Moosavi, Yadollah Yamini
Summary: Due to concern about health and the environment, green, eco, and environment-friendly practices have been established in different research areas. This has motivated the analytical chemistry community to improve methods that align with the principles of green analytical chemistry. Microextraction techniques, such as sorbent microextraction and liquid-phase microextraction, are of great importance as alternative methods. Parabens, synthetic preservatives widely used in cosmetics, pharmaceuticals, and beverages, are known as endocrine-disrupting chemicals. This review discusses the definition and principles of green chemistry, summarizes the development of green analytical chemistry, and focuses on recent applications for the determination of parabens in different samples.
TRAC-TRENDS IN ANALYTICAL CHEMISTRY
(2023)
Review
Biochemistry & Molecular Biology
Abuzar Kabir, Victoria Samanidou
Summary: Fabric phase sorptive extraction (FPSE) is a revolutionary sample preparation method that utilizes a chemically coated sol-gel organic-inorganic hybrid sorbent on a fabric substrate, resulting in a versatile, fast, and sensitive micro-extraction device. The user-friendly FPSE membrane allows direct extraction of analytes without sample modification, eliminating the need for time-consuming sample pre-treatment steps.
Review
Chemistry, Analytical
Raul Gonzalez-Martin, Adrian Gutierrez-Serpa, Veronica Pino
Summary: Ferrofluids are a type of tunable magnetic material consisting of magnetic nanoparticles suspended in a liquid carrier, commonly used in various applications; recently, they have been incorporated as extractant materials in magnetic-driven analytical sample preparation procedures, taking advantage of both the magnetic susceptibility of nanoparticles and properties of the liquid carrier to achieve better extraction performance.
Review
Chemistry, Analytical
Wojciech Wojnowski, Marek Tobiszewski, Francisco Pena-Pereira, Elefteria Psillakis
Summary: AGREEprep is a metric tool that prioritizes sample preparation, evaluating factors such as solvent, material, and reagent choices, waste generation, and energy consumption to calculate the final assessment score. The assessment procedure utilizes intuitive software to generate an easy-to-read information pictogram showing overall performance and threat structure.
TRAC-TRENDS IN ANALYTICAL CHEMISTRY
(2022)
Article
Chemistry, Multidisciplinary
Justyna Plotka-Wasylka, Wojciech Wojnowski
Summary: The study proposed a new metric based on GAC attributes for evaluating the green nature of analytical procedures. This metric expands on the green analytical procedure index by adding additional fields related to processes performed before the analytical procedure, and was used to evaluate analytical protocols for determining pesticides in urine samples. It is expected to gain attention and acceptance from the chemical community.
Article
Chemistry, Analytical
Gabriel Jimenez-Skrzypek, Cecilia Ortega-Zamora, Javier Gonzalez-Salamo, Javier Hernandez-Borges
Summary: This review article provides an overview of the development of miniaturized green analytical sample preparation procedures in the pharmaceutical analysis field, focusing on environmentally friendly solvents and sorbents, nanomaterials, and high extraction capacity sorbents. These methods significantly reduce solvent volumes and reagents amounts, offering advantages from a sustainability perspective.
JOURNAL OF PHARMACEUTICAL AND BIOMEDICAL ANALYSIS
(2022)
Review
Chemistry, Analytical
Meiyun Shi, Xinyue Zheng, Ning Zhang, Yufeng Guo, Meichen Liu, Lei Yin
Summary: Green analytical chemistry (GAC) is a concept widely recognized in analytical chemistry laboratories that promotes the use of energy-saving instruments, reduction of toxic agents, and minimal waste production. This article introduces and discusses 16 typical greenness metric tools, such as the National Environmental Methods Index (NEMI), Analytical Eco-scale, Analytical method volume intensity (AMVI), Green Analytical Procedure Index (GAPI), and Analytical Greenness Calculator (AGREE), including their criteria, characteristics, advantages, disadvantages, and applications. The aim is to help analysts assess the greenness of different analytical procedures using various metric tools.
TRAC-TRENDS IN ANALYTICAL CHEMISTRY
(2023)
Review
Chemistry, Analytical
Francesca Merlo, Antonella Profumo, Andrea Speltini
Summary: Steroid hormones, widely used in medicine, are also known as endocrine-disrupting chemicals due to their presence in water bodies. Various sample treatment protocols, particularly liquid- and solid-phase extractions, have been developed for their sensitive determination. Recent methods have simplified protocols and improved sample throughput, with further potential for overall impact. The AGREEprep tool highlights the strengths and weaknesses of selected procedures and assesses their environmental impact based on green sample preparation principles.
TRAC-TRENDS IN ANALYTICAL CHEMISTRY
(2023)
Review
Chemistry, Analytical
Belen Herce-Sesa, Jose A. Lopez-Lopez, Carlos Moreno
Summary: The incorporation of ionic liquids in LPME for metal extraction has shown great potential in sample preparation for environmental analysis. This has led to the development of more efficient and selective extraction methods, with the use of task specific ionic liquids and deep eutectic solvents. The future development of IL-LPME for metal extraction shows promise for further advancements in the field.
TRAC-TRENDS IN ANALYTICAL CHEMISTRY
(2021)
Article
Chemistry, Analytical
Muhammad Sajid
Summary: The development of greener and more efficient materials for extracting environmental contaminants is a growing area of research. Chitosan, enriched with amino and hydroxyl groups, is a non-toxic biopolymer that can be used for extracting pollutants and functionalizing with other materials. This review provides an overview of the applications of chitosan-based sorbents in analytical extractions and water treatment.
TRENDS IN ENVIRONMENTAL ANALYTICAL CHEMISTRY
(2022)
Article
Chemistry, Inorganic & Nuclear
Sk Safikul Islam, Rostam Ali Molla, Sabyasachi Ta, Nasima Yasmin, Debasis Das, Sk Manirul Islam
JOURNAL OF ORGANOMETALLIC CHEMISTRY
(2019)
Article
Chemistry, Physical
Susanta Adhikari, Sabyasachi Ta, Avijit Ghosh, Subhajit Guria, Abhishek Pal, Manisha Ahir, Arghya Adhikary, Sumit Kumar Hira, Partha Pratim Manna, Debasis Das
JOURNAL OF PHOTOCHEMISTRY AND PHOTOBIOLOGY A-CHEMISTRY
(2019)
Article
Chemistry, Multidisciplinary
Sabyasachi Ta, Milan Ghosh, Rostam Ali Molla, Subhasis Ghosh, Manirul Islam, Paula Branclao, Vitor Felix, Debasis Das
Article
Engineering, Environmental
Aparna Banerjee, Debasis Das, Shalini Gaur Rudra, Koushik Mazumder, Rodrigo Andler, Rajib Bandopadhyay
JOURNAL OF POLYMERS AND THE ENVIRONMENT
(2020)
Article
Chemistry, Applied
Sabyasachi Ta, Milan Ghosh, Noor Salam, Jayanta Das, Manirul Islam, Paula Brandao, Vitor Felix, Jesus Sanmartin, Debasis Das
APPLIED ORGANOMETALLIC CHEMISTRY
(2020)
Article
Engineering, Environmental
Aparna Banerjee, Debasis Das, Rodrigo Andler, Rajib Bandopadhyay
Summary: This study utilized exopolysaccharide (EPS) synthesized by B. anthracis PFAB2 from a geothermal spring to green synthesize silver nanoparticles (AgNPs), which exhibited good monodispersity and antimicrobial properties, showing potential for treating microorganisms resistant to traditional antibiotics or antifungal drugs.
JOURNAL OF POLYMERS AND THE ENVIRONMENT
(2021)
Article
Chemistry, Multidisciplinary
Mahuya Banerjee, Milan Ghosh, Sabyasachi Ta, Subhasis Ghosh, Debasis Das
NEW JOURNAL OF CHEMISTRY
(2020)
Article
Chemistry, Multidisciplinary
Priyanka Paul, Noor Salam, Aslam Khan, Debasis Das, Seikh Mafiz Alam, Sk Manirul Islam
NEW JOURNAL OF CHEMISTRY
(2020)
Article
Chemistry, Multidisciplinary
Ahad Shaikh, Milan Ghosh, Pallabi Mukherjee, Avijit Ghosh, Rostam Ali Molla, Sabyasachi Ta, Debasis Das
NEW JOURNAL OF CHEMISTRY
(2020)
Article
Chemistry, Multidisciplinary
Somnath Khanra, Sabyasachi Ta, Ankush Paladhi, Milan Ghosh, Subhasis Ghosh, Sumit Kumar Hira, Partha Partim Manna, Paula Brandao, Vitor Felix, Debasis Das
CHEMICAL COMMUNICATIONS
(2020)
Article
Chemistry, Multidisciplinary
Ahad Shaikh, Pallabi Mukherjee, Sabyasachi Ta, Arunasis Bhattacharyya, Abhijit Ghosh, Debasis Das
NEW JOURNAL OF CHEMISTRY
(2020)
Article
Chemistry, Multidisciplinary
Seikh Taniya, Somnath Khanra, Sabyasachi Ta, Sudeshna Chatterjee, Noor Salam, Debasis Das
Article
Chemistry, Multidisciplinary
Somnath Khanra, Sabyasachi Ta, Milan Ghosh, Sudeshna Chatterjee, Pallabi Mukherjee, Debasis Das
NEW JOURNAL OF CHEMISTRY
(2020)
Article
Chemistry, Multidisciplinary
Noor Salam, Priyanka Paul, Swarbhanu Ghosh, Usha Mandi, Aslam Khan, Seikh Mafiz Alam, Debasis Das, Sk Manirul Islam
NEW JOURNAL OF CHEMISTRY
(2020)
Article
Nanoscience & Nanotechnology
Mahuya Banerjee, Milan Ghosh, Sayantan Pradhan, Jesus Sanmartin Matalobos, Abhinandan Rej, Sumit Kumar Hira, Debasis Das
ACS APPLIED BIO MATERIALS
(2019)
Review
Chemistry, Analytical
Claudia Campanale, Silvia Galafassi, Francesca Di Pippo, Iulian Pojar, Carmine Massarelli, Vito Felice Uricchio
Summary: Biodegradable plastic mulches (BDMs) have the potential to be an eco-friendly alternative to conventional plastic mulches in agriculture. However, their long-term impacts on soil ecosystems are still uncertain, and further research is needed. Incorporating BDMs into the soil may stimulate microbial activity, but there is also a risk of incomplete degradation and release of residual microplastics and additives.
TRAC-TRENDS IN ANALYTICAL CHEMISTRY
(2024)
Review
Chemistry, Analytical
Xuechi Yin, Sijie Liu, Deepak Kukkar, Jianlong Wang, Daohong Zhang, Ki-Hyun Kim
Summary: The lateral flow immunoassay strip is a classic and dominant tool in point-of-care detection, known for its portability and simplicity. However, current colored nanomaterials used as signal labels in LFIA have limited sensing potential, leading to the recognition of composite nanoparticles as alternatives to enhance sensitivity, signal readout diversity, anti-matrix interference, and cost-effectiveness.
TRAC-TRENDS IN ANALYTICAL CHEMISTRY
(2024)
Review
Chemistry, Analytical
Yaxin Cao, Longyi Shao, Timothy P. Jones, Wenjing Deng, M. Santosh, Pengju Liu, Cheng-Xue Yang, Yaowei Li, Daizhou Zhang, Kelly Berube
Summary: The toxicity of fibrous particles in ambient air can be higher than other types of particles. Microfibers can be organic or inorganic and their presence in the atmosphere as a result of human activity raises concerns for environmental and public health. Accurate collection, identification, and understanding of the health hazards associated with these fibers are crucial for mitigation strategies and protection of public health.
TRAC-TRENDS IN ANALYTICAL CHEMISTRY
(2024)
Review
Chemistry, Analytical
Chenchen Xie, Chen Meng, Huilin Liu, Baoguo Sun
Summary: The development of food hazard factor (FHF) detection has been moving towards on-site inspection and mobile law enforcement, calling for simple, fast, and affordable analysis technology to ensure food safety and quality. This review comprehensively summarizes the progress in research on smartphone-assisted MIP optosensors, focusing on the key issues of accuracy and sensitivity.
TRAC-TRENDS IN ANALYTICAL CHEMISTRY
(2024)
Review
Chemistry, Analytical
Guillem Peris-Pastor, Cristian Azorin, Jose Grau, Juan L. Benede, Alberto Chisvert
Summary: Green Analytical Chemistry plays an important role in every stage of method development, including sample preparation. Extraction techniques have evolved from conventional ones to a variety of miniaturized techniques in order to enhance analytical performance and ensure safety for operators and the environment. Green metric tools are used to evaluate the impact and sustainability of methods, with AGREEprep selected as the most suitable tool for evaluating published methods in various applications. The miniaturization of sample preparation strategies has led to the use of less and safer solvents, reduced waste generation and energy consumption, and improved portability and throughput.
TRAC-TRENDS IN ANALYTICAL CHEMISTRY
(2024)
Review
Chemistry, Analytical
Helena Hruskova, Roman Reminek, Frantisek Foret
Summary: This review article summarizes the progress and recent studies in offline electromigration preparative techniques between 2018 and 2023. It covers various techniques including electrophoresis, free-flow electrophoresis, isoelectric focusing, and isotachophoresis, providing theoretical aspects, trends, and solutions to existing limitations in each technique.
TRAC-TRENDS IN ANALYTICAL CHEMISTRY
(2024)
Review
Chemistry, Analytical
Mayank Garg, Nicole Pamme
Summary: This review focuses on the removal strategies of templates from molecularly imprinted polymers (MIPs) used in diagnostic biosensors. Chemical-based and electrochemical-based template extraction approaches are summarized and evaluated, providing guidance for researchers in the fields of analytical chemistry, diagnostics, and materials science for the design of MIP-based sensors.
TRAC-TRENDS IN ANALYTICAL CHEMISTRY
(2024)
Review
Chemistry, Analytical
Ivneet Banga, Anirban Paul, Nathan Kodjo Mintah Churcher, Ruchita Mahesh Kumar, Sriram Muthukumar, Shalini Prasad
Summary: Breathomics is an emerging field that focuses on analyzing exhaled breath to diagnose and monitor respiratory diseases. Electrochemical sensors, with their high sensitivity, selectivity, and low cost, play a significant role in breathomics and can be integrated into portable devices for point-of-care diagnosis.
TRAC-TRENDS IN ANALYTICAL CHEMISTRY
(2024)
Review
Chemistry, Analytical
Fabjola Bilo, Paola Cirelli, Laura Borgese
Summary: This review explores the application of X-ray fluorescence (XRF) spectrometry for elemental analysis of particulate matter (PM) in air quality monitoring. It discusses the fundamentals of XRF, experimental configurations, PM sampling devices and substrate, sample preparation strategies, qualitative and quantitative analysis, as well as the challenges faced by XRF in becoming a reliable analytical technique for PM analysis.
TRAC-TRENDS IN ANALYTICAL CHEMISTRY
(2024)
Review
Chemistry, Analytical
Hakim Faraji
Summary: The dispersive liquid-liquid microextraction (DLLME) technique is widely popular in analytical chemistry due to its high efficiency, cost-effectiveness, and simplicity. Recent advancements have addressed the limitations of DLLME, incorporating greener solvents, innovative dispersion strategies, and simplified procedures. These changes have made DLLME a more sustainable and efficient technique.
TRAC-TRENDS IN ANALYTICAL CHEMISTRY
(2024)
Review
Chemistry, Analytical
Sherin F. Hammad, Inas A. Abdallah, Alaa Bedair, Reda M. Abdelhameed, Marcello Locatelli, Fotouh R. Mansour
Summary: Carbon nanomaterials (CNMs) have excellent capabilities in terms of adsorption, enhanced oxidation, and photocatalysis, attracting widespread attention in different fields. Metal-organic frameworks (MOFs) have been widely used due to their regular network structure, porous nature, and large specific surface area. However, the instability of MOFs in aqueous solutions limits their applications in chemical sensing. Recent studies have focused on increasing the stability of MOFs in water-based matrices through chemical modifications using CNMs.
TRAC-TRENDS IN ANALYTICAL CHEMISTRY
(2024)
Review
Chemistry, Analytical
Alexandra Pape, Oliver J. Schmitz
Summary: Low temperature plasmas based on dielectric barrier discharges have emerged as a recent development in ion source research. These ion sources are applicable to heat-sensitive analytes and can ionize a wide range of compounds. Despite intensive research on important parameters such as configuration, shape, size, and materials in the past two decades, the actual ionization mechanism for all plasma gases has not been fully elucidated. This review provides an overview of atmospheric pressure ion sources, with a focus on plasma and dielectric barrier discharge based ion sources, summarizing the reactions occurring in the plasma and discussing the applications developed by different research groups.
TRAC-TRENDS IN ANALYTICAL CHEMISTRY
(2024)
Review
Chemistry, Analytical
Hai Xiong, Fengli Li, Linyu Zeng, Qiyu Lei
Summary: This review provides an overview of the emerging trends in the use of functional COF nanomaterials as biosensors for DNA/RNA detection. It summarizes the construction of DNA/RNA hybridized COF nanoprobes and their potential applications in bioanalyte detection, biosensing, biomarker imaging, and clinical biomedicine.
TRAC-TRENDS IN ANALYTICAL CHEMISTRY
(2024)
Review
Chemistry, Analytical
Bing Yan
Summary: This article summarizes the recent progress in logic gate computing and operation based on multiple luminescence response and chemical sensing for lanthanide functionalized MOF hybrid systems. The article first describes multi-color luminescence and the subsequent multiple luminescence response. The basic concept of logic gate operation and the advantages of lanthanide-based hybrid materials are then introduced. Reports on logic gate operation using pure lanthanide MOFs are provided, followed by a detailed summary of logic gate operations using lanthanide functionalized MOF hybrid materials. Additionally, the article discusses the practical luminescent detection of analytes by correlating the luminescence responsive signals and the concentration of different analytes. Finally, the article concludes with a prospect for this topic.
TRAC-TRENDS IN ANALYTICAL CHEMISTRY
(2024)
Review
Chemistry, Analytical
Brij Mohan, Gurjaspreet Singh, Rakesh Kumar Gupta, Pawan Kumar Sharma, Alexander A. Solovev, Armando J. L. Pombeiro, Peng Ren
Summary: Porous materials, particularly hydrogen-bonded organic frameworks (HOFs), have gained significant attention due to their versatile applications and unique properties such as well-defined crystalline structure and easy regeneration processes. This article provides a comprehensive overview of HOFs, including synthesis methods, hydrogen bonding motifs, recent advancements, and potential applications, offering valuable guidance for further exploration in this dynamic field.
TRAC-TRENDS IN ANALYTICAL CHEMISTRY
(2024)
