期刊
TETRAHEDRON LETTERS
卷 52, 期 11, 页码 1217-1221出版社
PERGAMON-ELSEVIER SCIENCE LTD
DOI: 10.1016/j.tetlet.2011.01.039
关键词
PTP inhibitors; Direct alpha-halogenation; Chlorotrimethylsilane; Nitryl chloride; Density functional theory
资金
- Loker Hydrocarbon Research Institute
A mixture of chloro/bromotrimethylsilane and nitrate salt is found to be an effective reagent system for the alpha-chlorination/bromination of carbonyl compounds. The reaction occurs under mild conditions yielding the products in moderate to good yields. (C) 2011 Elsevier Ltd. All rights reserved.
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